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help crystalizing? Options
 
chemisch
#1 Posted : 2/17/2013 10:48:25 PM

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Last visit: 21-May-2013
Location: washington
My workspace isnt exactly humidity free, its a large shed basically. i performed a acid base extraction acetic acid as the acid lye as the base and did my pulls with DCM, i was left after evaporation with a slightly reddish goop it. its dmt after a volcano vape bag i was in dmt land any ideas for my next pulls to make sure it crystallizes i was thinking making a vacuum chamber to suck the moisture out? or washing it something?
if you can bassify in ammononia and extract with dcm why not smoke it?
 

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SnozzleBerry
#2 Posted : 2/17/2013 11:29:52 PM

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Moderator | Skills: Growing (plants/mushrooms), Research, Extraction troubleshooting, Harmalas, Revolution (theory/practice)

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Re-x with heptane (or even naphtha). Afaik, DCM pulls more fats/oils than naphtha, like xylene, toluene, limonene, etc.
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chemisch
#3 Posted : 2/17/2013 11:42:33 PM

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Location: washington
i love how quickly dcm evaporates and recrystallizing isnt to fun, defatting thoroughly with dcm or chloroform because they are so similar that would stop this issue correct? chloroform preferably bleach is quite cheap
if you can bassify in ammononia and extract with dcm why not smoke it?
 
 
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