We've Moved! Visit our NEW FORUM to join the latest discussions. This is an archive of our previous conversations...

You can find the login page for the old forum here.
CHATPRIVACYDONATELOGINREGISTER
DMT-Nexus
FAQWIKIHEALTH & SAFETYARTATTITUDEACTIVE TOPICS
Pure mdma separation Options
 
space face
#1 Posted : 1/23/2013 9:24:29 PM
AND THIS IS WHY!


Posts: 66
Joined: 25-Jan-2012
Last visit: 06-Nov-2019
Location: Michigan
Hey everybody!

I have some mdma+fiber supplent powder

Any idea on how I can remove the fiber so I have pure mdma?

I currently have naphtha, xylene, and isoproyl alcohol if those could be used as potentiol solvents

I tested it with a marquis reagent acquired from dance safe. Stuff turned instantly black Very happy

I know the other ingredient is fiber because the genius who added it told meThumbs down
Thanks people

-space face
Learn. Manifest. Integrate. Grow.
 

Good quality Syrian rue (Peganum harmala) for an incredible price!
 
Ambivalent
#2 Posted : 1/23/2013 9:59:28 PM

DMT-Nexus member


Posts: 336
Joined: 01-Jul-2011
Last visit: 29-Jun-2024
Location: Gaia
the mdma is usually sold in salt form. and the salts afaik are not soluble in non polars like naphtha and mixed hydrocarbons.maybe you should try to wash it with a non polar solvent. or try to find out what is that supplement powder soluble in. or maybe just try to dissolve a small ammount in water and see if everything dissolves.

edit : i missread about the fiber suplement powder so i re edited my post.
 
space face
#3 Posted : 1/24/2013 12:01:50 PM
AND THIS IS WHY!


Posts: 66
Joined: 25-Jan-2012
Last visit: 06-Nov-2019
Location: Michigan
Thanks for the reply. That's good to know mdma isn't soluble in non polar solvents. Ill be doing as you said and continue researching to find what that supplement powder could possibly be soluble in, and then do some sort of wash based on my results.
Thanks for that input it's appreciated
-space face
Learn. Manifest. Integrate. Grow.
 
Ambivalent
#4 Posted : 1/24/2013 12:32:58 PM

DMT-Nexus member


Posts: 336
Joined: 01-Jul-2011
Last visit: 29-Jun-2024
Location: Gaia
space face wrote:
mdma isn't soluble in polar solvents.
-space face


maybe you made a typo but just to be sure its non polar solvents that aren't dissolving the salts.
 
Infundibulum
#5 Posted : 1/24/2013 12:59:44 PM

Kalt und Heiß, Schwarz und Rot, Kürper und Geist, Liebe und Chaos

ModeratorChemical expert

Posts: 4661
Joined: 02-Jun-2008
Last visit: 30-Apr-2022
space face wrote:
Thanks for the reply. That's good to know mdma isn't soluble in polar solvents. Ill be doing as you said and continue researching to find what that supplement powder could possibly be soluble in, and then do some sort of wash based on my results.
Thanks for that input it's appreciated
-space face

Spaceface, just dissolve the mdma it in water, then evaporate water.

The fibres should not dissolve in water, but then again it depends on the type of fibres; if you got no clue what these fibre additives they are, then it is impossible to pick a solvent that would be selective for mdma only. But your first guess would be fibres are insoluble in water, while mdma is soluble in water (water is an extremely polar solvent).

You can always evaporate the water and get your starting material if everything dissolves (that is, both mdma and fibres) to get your starting material. Even better, why don't you save yourself the trouble and ask the guy how much fibre did he add? that way you can adjust your dose accordingly.


Need to calculate between salts and freebases? Click here!
Need to calculate freebase or salt percentage at a given pH? Click here!

 
space face
#6 Posted : 1/24/2013 1:00:30 PM
AND THIS IS WHY!


Posts: 66
Joined: 25-Jan-2012
Last visit: 06-Nov-2019
Location: Michigan
Oh whoops good catch! It's early for me right now lol.. Fixed it
Learn. Manifest. Integrate. Grow.
 
space face
#7 Posted : 1/24/2013 1:06:28 PM
AND THIS IS WHY!


Posts: 66
Joined: 25-Jan-2012
Last visit: 06-Nov-2019
Location: Michigan
Infundibulum wrote:
space face wrote:
Thanks for the reply. That's good to know mdma isn't soluble in polar solvents. Ill be doing as you said and continue researching to find what that supplement powder could possibly be soluble in, and then do some sort of wash based on my results.
Thanks for that input it's appreciated
-space face

Spaceface, just dissolve the mdma it in water, then evaporate water.

The fibres should not dissolve in water, but then again it depends on the type of fibres; if you got no clue what these fibre additives they are, then it is impossible to pick a solvent that would be selective for mdma only. But your first guess would be fibres are insoluble in water, while mdma is soluble in water (water is an extremely polar solvent).

You can always evaporate the water and get your starting material if everything dissolves (that is, both mdma and fibres) to get your starting material. Even better, why don't you save yourself the trouble and ask the guy how much fibre did he add? that way you can adjust your dose accordingly.



Yes this is what ill be doing^. Frankly he told me he tried to just "cut it a little" , but ended up adding more than he intended, about 50/50..
I just don't trust it being that there's anything else in it at the moment at all.. Aquaintences have taken 240 mg and noted it felt exactly like around 100 mg of moonrocks but I'd rather just get that other stuff out altogether.It's frustrating when people do these things..
Learn. Manifest. Integrate. Grow.
 
dg
#8 Posted : 1/25/2013 2:45:05 AM
DMT-Nexus member

Cacti expert

Posts: 1175
Joined: 10-Jun-2010
Last visit: 27-Dec-2024
water and filter is probably easiest

sexy crystals can be grown in minimal water and acetone (or other solvent mixes)
 
infinitynlove
#9 Posted : 1/25/2013 6:48:49 AM

Mushroom Explorer


Posts: 538
Joined: 18-Jan-2013
Last visit: 19-Aug-2024
Location: Mushvile
could he basify and extract with a none polar solvent?
I am certifiably insane, as such all posts written by me should be regarded as utter nonsense or attempts to get attention in fact everything I write here is a lie !

I hope in some way, my posts and replies may of helped you, I hope you like what I have said here if not feel free to send me a none flame PM
 
 
Users browsing this forum
Guest (2)

DMT-Nexus theme created by The Traveler
This page was generated in 0.018 seconds.