Once you got it, you never forget it, it gets easier, and you get better at it evry time you do it.
Pic 1&2 is after 1 hour in the refridgerator.
Pic 3 is after 6 hours in the freezer.
Lesson learned hear folks is that if your solvent is spice rich you wont have to even put it in the freezer to get it to precip out.
The spice rich solvent was never left to evap before cooling. The secret to getting the solvent so spice rich? I let it soak for a solid month at room temp, 72 deg Far.
Not sure how much spice is in this 3d pull from a 600gm mhrb evolution I suspect a solid gram or more. Solvent used, heptane. Base used, NAOH.
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