We've Moved! Visit our NEW FORUM to join the latest discussions. This is an archive of our previous conversations...

You can find the login page for the old forum here.
CHATPRIVACYDONATELOGINREGISTER
DMT-Nexus
FAQWIKIHEALTH & SAFETYARTATTITUDEACTIVE TOPICS
acetone freeze precip mesc? Options
 
mew
#1 Posted : 10/12/2012 6:52:54 AM

huachumancer


Posts: 1285
Joined: 02-Aug-2008
Last visit: 21-Sep-2024
Location: earf
swimew was cleaning some hcl with dry acetone and as usual it boiled acetone with the hcl in it ( it assumes this increases the cleaning ability of acetone with less manual labor) however when it set the vessel on an angle to let the hcl settle in a corner it noticed (upon returning when it cooled to rt) some white flakes suspended in the acetone some seemed to be square shards, so it put the vessel in the fridge and noticed a slight increase in the amount of floating white shards.

the rest of the mesc was dark tan as it typically use too much hcl when salting, but these shards were close to white. mew is wondering if some portion of the mesc alkaloids are soluble in boiling acetone, as it would seem. mew cant upload a decent picture as his camera is too low grade


anyone else have experience with this?


perhaps this is the mystery hcl substance, it will be isolated and tested for solubility in water, if it is insoluble in water and dry ipa then it may be mews mystery hcl substance. if not, then it will be assayed and the results noted.
 

Good quality Syrian rue (Peganum harmala) for an incredible price!
 
AlbertKLloyd
#2 Posted : 10/14/2012 8:27:45 AM

DMT-Nexus member


Posts: 1453
Joined: 05-Apr-2009
Last visit: 02-Feb-2014
Location: hypospace
no first hand with the method, but the squarish shards sound right, I've seen that and needle like shapes and mixes between the two
 
Kash
#3 Posted : 10/17/2012 7:30:51 PM

DMT-Nexus member

Senior Member | Skills: Chemistry and Programming

Posts: 833
Joined: 19-Oct-2010
Last visit: 21-Aug-2023
Location: Planet Earth
Cool mew, maybe that was some hcl that dissolved in the hot acetone and then preciped out. Have they tested bitter?
--------------------------------------------------*Kash's LSA Extraction* * Kash's Mescaline Extraction*------------------------------------------------------
All things I say are complete and utter ramblings of nonsense. Do not consider taking anything iterated from the depths of my subconsciousness rationally and/or seriously.
 
 
Users browsing this forum
Guest

DMT-Nexus theme created by The Traveler
This page was generated in 0.012 seconds.