I did FASA precip from d-limonene with mimosa alkaloids recently. The limo and the FASA mixed well, no separate layers. I started by adding just a few drops every minute or so. The clouding didn't sink at all, so i started adding larger gulps, and the FASA thinned the limo enough for (most of) the precipitate to sink to the bottom. I recovered the ultra-fine floating fumarate in a coffee filter, and scraped the crystals from the bottom.
(Edit: The light in the right half of the precipitating pic is not UV, it's just colored LED to make the cloud more visible)
Homo Trypens attached the following image(s):
precipitating.jpg
(958kb) downloaded 78 time(s). shades.jpg
(447kb) downloaded 78 time(s).