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Removing N - Oxide from old bark Options
 
Dwhitty76
#1 Posted : 1/24/2009 7:33:50 PM

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Swim has powdered bark thats been sitting around for about 6 -9 months and is want's to get rid of any oxidation to improve yields.

I saw a thread a while back, in which 69Ron gave a good summary on how to remove the n-oxide and then go on w/ the normal extracton. I cant find that thread, does anyone know of it's location.

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Entropymancer
#2 Posted : 1/26/2009 6:24:09 AM

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The thread you're thinking of is DMT N-oxide to Freebase DMT.

The DMT in 9 month old bark is not likely to have oxidized much, but you could try and see if it makes a difference.
 
Observant
#3 Posted : 1/26/2009 3:21:08 PM

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Please post your Results if you give it a try !
Had he more quickly realized just who they were,he would have shown them more respect.Had he tried harder to fathom their brilliant minds,he would have taken more of their teachings to heart.Had he more clearly understood the purpose of their being,
he would have more vigorously tried to assist them.They were truly honorable; he was sadly prejudiced.
They were exceedingly well informed; he was grossly ignorant.They were totally indefatigable; he so often, and so quickly,gave up. Still, for many years there was a strong inter-species alliance between the Eleven-Eleven of the Half-way Realm, their Seraphic Associates,and their flesh-and-blood friend, a common mortal. Much was accomplished, many profited, and, there’s only one regret...They could have achieved so much more...

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Dwhitty76
#4 Posted : 1/27/2009 8:40:38 PM

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Thanx Entropymancer, i saw the thread a while back but couldnt find it.

I will post results, if swim gives it a go.
Smile
" Freedom from the desire for an answer is essential to the understanding of a problem." - jiddu Krishnamurti
 
acolon_5
#5 Posted : 1/27/2009 8:51:32 PM

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Probably a lot easier and more efficient to convert with elemental zinc or ascorbic acid before extraction and/or remove from your final product via recrystalization in heptane/hexane (oily yellow goo is possibly oxides and oils).
The Spice extends life
The Spice expands consciousness
The Spice is vital for space travel
___________________________________________________________________________________________________
Never underestimate the power of STUFF!


I am certifiably insane, as such all posts written by me should be regarded as utter nonsense or attempts to get attention.

I don't know SWIM and personally don't trust him at all. If SWIM is posting, most likely I will not respond...as I said, I don't trust the guy. YOU I trust, but never SWIM.
 
 
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