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freeze percip queery Options
 
notapillow
#1 Posted : 12/13/2008 10:38:50 PM
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Stop

sooooo
swim has taken 480g bark

put it into 4 gallon jugs


and rolled each with 125 ml naptha

toook the resulting 2000ml of naptha, evaped it down to about half (maybe a bit more)

and put the remaining loaded solvent into jars in the freezer

after one night only small flecs and dots of dmt have appered.

should swim wait, see what develops

he was gonna let it go for 2 days



or should he put it back in a pan and evap more in hopes of getting a more concentrated solution


any help would be gratefuly accepted

swim has been out of the game for a bit and wants to be sure he has not fucked up his first round back in the ring


thanksVery happy
 

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Jorkest
#2 Posted : 12/13/2008 10:40:27 PM

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way too much naphta..depending on how much you are using...but if you are extracing from say..100g of bark...2000ml is WAYYY too much..you only NEED to use 50 or so...100 is a bit better...but 2000 is way way way too much
it's a sound
 
notapillow
#3 Posted : 12/13/2008 10:43:39 PM
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using 120 grams in each jar
4 pulls on eac o the 4 jars results in about 2000ml


2000ml for almost 500g of bark dosent seem bad

i tryed to half it

thinking it would be concentraited enuf


maybe i sould have let it go more ?
 
Entropymancer
#4 Posted : 12/13/2008 10:47:32 PM

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It's still probably too dilute. I'd let it evap down to ~300 mL and then try to freeze-precip
 
notapillow
#5 Posted : 12/13/2008 10:55:10 PM
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cool

thanks budday!

back in fron of the fan you go



the only thing i was worried about was over drying (wich i did once before) where crystals started forming on part of the tray while naptha as still around



again thanks
 
Jorkest
#6 Posted : 12/13/2008 11:27:53 PM

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its ok if that happens..all that means is that the solution became to concentrated so crystals had to form...that is completely fine...you can even throw that in the fridge and have great results
it's a sound
 
notapillow
#7 Posted : 12/13/2008 11:31:26 PM
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oh i know its fine

i mean its a good thing

i just wish i had caught it a bit earlyer
cus its hard to get off the plate and back into naptha
 
Jorkest
#8 Posted : 12/13/2008 11:47:39 PM

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get a bit of acetone to clean off the glass..then evaporate it for some sweet stuuf
it's a sound
 
notapillow
#9 Posted : 12/13/2008 11:53:12 PM
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hmm
thats a good ider

do u just need to like swish it around in there
previouly when this happened to swim he just scraped up the .2 or so of oily evaped crystals and just added them to a later recrystalisation

swim just kinda wants to get the solution down just right so he can know for the future when its ripe to go in the freeer


hes been taking it from 2 pyrex trays. combinign the 2 after some evap

then evaping more

so he is aiming for almos like an 1/8 of original liqid
 
notapillow
#10 Posted : 12/14/2008 3:38:24 AM
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he got it down to about 400ml i would say
it fits in one jar now


crystals where aperent floating around in the liquid so h decided it had reached a good point




fingers crossed Smile
 
Faust
#11 Posted : 12/29/2008 8:16:39 PM

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notapillow wrote:
using 120 grams in each jar
4 pulls on eac o the 4 jars results in about 2000ml


2000ml for almost 500g of bark dosent seem bad

i tryed to half it

thinking it would be concentraited enuf


maybe i sould have let it go more ?

You are supposed to keep using and recycle each pull of Naptha, darling over and over again, not add them up all at once. Because at the end you will find that even after 6 or more freeze precips there is still DMT left hanging around; the naphtha can still hold on to a lot of it. SWIM's done 6 freeze-precips and spice keeps falling out consistently, even though now it is about 1/3 of the volume of the first pull.

It is much harder to get nice xtals from a big jar of the stuff than it is to get them from small little pools. DMT falls out of the smaller jars of naphtha much more quickly. You are supposed to re-use your solvent each time lol. That makes it a lot easier on you. Never throw anything away!
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notapillow
#12 Posted : 1/7/2009 12:44:18 PM
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swim has been recyceling naptha

but due to many things
time constraints
freezer space

other creatures sharing living spaces

swim couldent do ultiple jars or pulls

that would be desirable tho
 
notapillow
#13 Posted : 1/9/2009 6:34:03 PM
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hmmmm

another queery

if SWIM WAS to add up all the naptha pulls . then evap it down to a more useable concentration. If she put the resulting soulution in several small jars there would be more surface area for persipitation. as well as easyer reach for grabing the xtals.


does that sound sound???
 
 
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