How did SWIY recover the spice? It's virtually impossible that the material you obtained had much lye, and it certainly wasn't entirely lye. Since it was white, there's little it could have been besides spice. If SWIY freeze-precipped, it's virtually certain it was spice.
The biggest reason for people having misfires on their first attempts to smoke the spice is improper smoking technique (too much heat, destroying the spice instead of vaporizing). Also, some people probably naturally require a larger dosage.
Quote:SWIM'er has no amonia for recrystal atm
Ammonia for recrystallizing??? I don't follow. You recrystallize with heptane ideally, or naphtha less ideally.
Quote:now considering a jungle extract but quite confused. What is understood is that a STB tek can be followed with using xylene/touluene as the nonpolar solvent.
This is correct, xylene or toluene will pull the additional alkaloid(s)
Quote:Or is it freeze precipitated in naphtha and then evaporated in xylene?
Evaporated in xylene? I don't understand.
Quote:Would like to pull a tan wax out of the arse but not quite sure how its obtained
As far as I know, there is no way to control which "jungle spice" material you end up with. The binary solvent mix of ether and heptane sounds like the most likely to isolate the tan material, but most SWIMmers don't have access to diethyl ether (and it can be dangerous if it's old, or handled by someone not taking reasonable safety precautions)
All other methods of pulling jungle spice will pull whatever material they pull, it could be red, tan, or a mix.
I still am not sure I understand your FASA question:
60cc.oz wrote:Quote: A. Do an A/B or an STB on some plant material using any other teks that can be found around. In the case one chooses to do A/B no defatting of the acidic solution is really necessary.
B. Make the first pull using xylene/toluene. After the layers have separated, withdraw the xylene/toluene.
C. Add FASA dropwise in the xylene/toluene pull. One cannot add too much FASA. On the contrary, it is advised to add more FASA than necessary, just in case. Immediately clouds of precipitation will form. This is DMT-fumarate.
Does this mean that FASA will substitute the lye solution or STB using lye/xylene?
FASA is added
after doing a normal extraction (STB or A/B) ith xylene as the solvent. Once you have the xylene containing jungle spice, FASA is added dropwise to precipitate these alkaloids out (along with DMT)