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mesc carb wash? Options
 
Frac7alt1m3
#1 Posted : 7/14/2011 9:42:22 PM

DMT-Nexus member


Posts: 98
Joined: 07-Apr-2011
Last visit: 16-Dec-2022
im sorry if this is answered somewhere but even so i am the type that needs to be told
directly and in detail about something i have little experience in and i have a hard time looking though pages and pages of stuff.

so last night i spent about 6 hours brewing 60 grams of achuma in water.
then i started evaporating my final product of all the pulls and thought why not throw the rest to the achuma in some IPA.
so while evaporation i decided to start throwing in some of what i was pulling from the IPA which was noticeably the very last of whatever was left in the cacti.

pretty dumb i know but last time i "extracted" mesc i used only IPA and when i went to evaporate it all down
my jar broke and the alch mixed in with a bunch of water.

BUT a few days later i decided to evap the pretty hefty amount of water/alch and after spilling some outside i ended up with about 6 grams of mescaline carbonate(tar) from 50 grams of san pedro.
i ate 4 grams and it was effective.

the rest i used later when my friend found this process of putting vinegar with the carbonate and then pulling with acetone.
inconclusive on results. i just got a small amount of this goop.
perhaps i will try it again, but i hear mesc acetate isn't preferable.

so anyways i evap my achuma down and ended up with some nasty stuff again as expected.
the reason i didn't use alch this time is because i didn't want to eat the nasty crap and i know the tea resin would be easier on the stomach and my stomach cant handle anything anymore.
but i messed that up purposely.

so now i am left with about 22.5 grams of this tar, which is a lot more in comparison to my last one.

can someone direct me or tell me how i can reduce/wash/clean this stuff?

if i didn't have powder i would of just used houses tek
and if i had sufficient funds i would just take the time to extract it using phlux's, 69ron's tek or something


thanks







 

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mew
#2 Posted : 7/17/2011 6:11:19 AM

huachumancer


Posts: 1285
Joined: 02-Aug-2008
Last visit: 21-Sep-2024
Location: earf
aight buddy here you go...

take your tar and throw it at a homeless man claiming it to be god or....


put tar in pyrex open deep dish (pyrex for the exothermic reaction, deep dish for splatter control and housing liquid)

add dry lye

add minimal water to bassify alkaloids

stir into homogenous solution of syrupy goop

add NPS, and swirl

watch the nps get funkified, if nothing changes in the color of the NPS, pour it off (save it!) and add more lye/water and mix it into the tar for a higher ph to ensure the mescaline has been freebased

add the NPS again, swirl again

isolate nps

pull nps with acid solution (10 ml 30% hcl diluted with 50 ml distilled water, this is enough for 2 salts) (or distilled white vinegar)

let salts precip/separate for 15 minutes after vigorous mixing

swirl one more time to collect salts in aqueous layer (bottom layer)

separate salts and evaporate

OPTION 1 - enjoy dirty acetates or clean with some technique you find
OPTION 2 - take your dirty hydrochlorides and wash in cold anhydrous acetone, pour through thick cotton filter, take cotton filter and add 15 ml hot water to dissolve the clean captured mescaline onto an evaporation dish, evaporate and really enjoy ( i prefer a gram, nothing less ) save cotton filter for further use or repeat the hot water dissolving to ensure all product is retrieved


peace bra!
 
mew
#3 Posted : 7/17/2011 6:13:04 AM

huachumancer


Posts: 1285
Joined: 02-Aug-2008
Last visit: 21-Sep-2024
Location: earf
i neglected to mention you want to salt it 3 times minimum, 5 times is most, and 4 is the number between the two, and 1 is before 2 and after 0... case you didnt know
 
 
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