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philaris and fat Options
 
jakid
#1 Posted : 1/11/2011 4:15:47 AM
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SWIM has done a few extrations from acacia with no de-fatting problems
but SWIM is trying to do a pull from phillaris (a/b). the more shellite that is added, the more fat comes out. so after 4-5 times of de-fatting SWIM whent to the next step to bassify the solution. but the problem was - there was still FAT in the sovent!!!
my question is, how can SWIM remove the fat from the acidified phalaris solution??
 

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endlessness
#2 Posted : 1/11/2011 10:24:00 AM

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Maybe forget de-fatting and instead crash the fumarates out of the solvent and later convert to freebase and recrystallize if necessary?
 
 
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