here is the run down on what was done.

following this tek as a very fast lazy version, swim is not as patient.
https://www.dmt-nexus.me....aspx?g=posts&t=8660


some acacia bark was blended up to smaller pieces. call it "rough powder".

30g weighted and put in a bowl with 50ml vinegar.

put in hot water bath for 15 mins

add 50g (dry) lime powder and about 40ml after all said and done.

stir/mix for 10 mins

add about 40ml zippo fluid...no naptha handy at the time.

3 pulls of same amount while soaked 15 mins each time. put in bowl and put in freezer. all is greta, crsytals from, large ones, within 10 mins.

next morning, swim pours off the liquid as much as one can and leaves bowl to dry under fan...but all crystals melt right away.

what can one do to avoid this...? or fix it. swim did grab a couple bogger ones and place on a pre weighed piece of foil and tried it, was certainly very much spice. but cant keep it in solid form

swim said she wants to try larger extractions, using kg's of bark (with real naptha) but doesnt want to get into it until this is figured out.

First place to check is the FAQ

https://wiki.dmt-nexus.m...ystals_after_freezing.3F

Why do you want to extract kgs of bark though? Why needing that much dmt?

From what I've read of acacia, there are a lot more plant oils and fats to deal with than with MHRB.
Melted into what? Likely the plant crap solidified in the freezer and when it warmed up it turned back into liquid.
Taking the DMT with it.
The alks should be in there.
Along with whatever the fine people at Ronsonal decided to lubricate their Zippos with that day.