Hi again, could someone please better explain two of these steps in Jorkest's bufo extraction.
Step 3 ) Prepare your FASA by adding your 1g of fumaric acid to 150ml of acetone, and stir. Add the FASA to the 600ml of filtered Acetone, for the Bufotenine to fumarate salt conversion, which will settle to the bottom. Continue adding FASA until clouds no longer form in the mixture. Pour out the Acetone/FASA mixture after all solids precipitate and keep the left-over solids. (SWIM just needs to know what the solids that precipitate out will look like)
AND
Step 7 ) Pour off the boiling D-limonene into a dish with a large surface area so that it can cool. When pouring off the D-limonene you have to wait until it stops boiling, this only takes like 5 seconds because otherwise the contaminates do not puddle up. After it stops bubbling immediately pour it off because it is starting to drop the bufotenine. As soon as the D-limonene cools below itβs boiling point, Bufotenine freebase will quickly fall out of it; emphasis on quickly! It happens in mere minutes. Allow the D-limonene to continue to cool completely and then pour off the remaining clear d-limonene. You should be left with approximately 1g of Bufotenine freebase, allow residual d-limonene to evaporate off, using a slightly warm hotplate speeds this up greatly. (SWIM is confused about, Allow the D-limonene to continue to cool completely and then pour off the remaining clear d-limonene.)