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First Time Recrystallizing - 3-4 Grams of Yellow & Orange DMT Options
 
CrushNazT
#1 Posted : 5/8/2010 9:44:53 PM

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Good quality Syrian rue (Peganum harmala) for an incredible price!
 
CrushNazT
#2 Posted : 5/8/2010 9:47:40 PM

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CrushNazT
#3 Posted : 5/8/2010 9:53:04 PM

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CrushNazT
#4 Posted : 5/8/2010 10:47:58 PM

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Ice House
#5 Posted : 5/8/2010 11:53:39 PM

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Right on! Your on the right track. Looks like you've done your homework. Keep it up. Cant wait to see some final xtal pics.
Ice House is an alter ego. The threads, postings, replys, statements, stories, and private messages made by Ice House are 100% unadulterated Bull Shit. Every aspect of the Username Ice House is pure fiction. Any likeness to SWIM or any real person is purely coincidental. The creator of Ice House does not condone or participate in any illicit activity what so ever. The makebelieve character known as Ice House is owned and operated by SWIM and should not be used without SWIM's expressed written consent.
 
CrushNazT
#6 Posted : 5/9/2010 12:55:27 AM

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Gir
#7 Posted : 5/9/2010 1:22:08 AM

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Mckenna says he used to smoke orange dmt.

Might want to put a bit aside and try it (like SWIM did this afternoon before he re-xd. boy was he glad he saved a bit ^.^)
Lets go extract something together Smile

house wrote:
19:10:05 ‹house› mama aya gave me lego man eye healers


Smoke Spice, NOW

Gir likes to tell lies, and the truth, but gir cant even tell the difference between them...


http://www.thevenusproject.com/index.phpTHIS IS THE VENUS PROJECT.
 
CrushNazT
#8 Posted : 5/9/2010 1:32:50 AM

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CrushNazT
#9 Posted : 5/9/2010 1:49:42 AM

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HyperD
#10 Posted : 5/9/2010 4:12:46 PM

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Nice
I would save some of that orangeVery happy




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CrushNazT
#11 Posted : 5/9/2010 6:10:39 PM

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dell500
#12 Posted : 5/14/2010 8:33:09 PM

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Did the same process. Thanks Crush! Workin' great.
 
criticalhalt
#13 Posted : 9/23/2010 12:24:31 PM
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If I were to use bestine instead of naptha would there be any difference in the procedure?
 
gibran2
#14 Posted : 9/23/2010 2:15:07 PM

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Here’s an even better way to clean up really dirty spice:

---- Put impure DMT into a jar used for extraction.

---- Add enough vinegar to dissolve all DMT.

---- Add water to increase volume (many impurities will stay in the water).

---- Prepare a small amount of NaOH solution.

---- Add NaOH solution to DMT solution – DMT will immediately precipitate.

---- Extract freebase in the usual manner.
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ucorky
#15 Posted : 9/23/2010 4:36:31 PM
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I like this. I think.
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criticalhalt
#16 Posted : 9/24/2010 3:20:30 AM
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@gibran2

I think I will try your method for recrystallization next. I had two questions:

How much water do you add to the vinegar/dirty spice solution? For example 1/2 the same or 2X the amount of vinegar.
What is in the NAOH solution? Is it just water and NAOH?
 
mumbles
#17 Posted : 9/24/2010 3:31:34 AM

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criticalhalt he is just describing another acid/base extraction. Volumes are entirely up to you as long as everything is dissolved. Yes an NaOH solution is just NaOH and water. Always add the base to the water and use goggles/gloves.
 
gibran2
#18 Posted : 9/24/2010 3:46:03 AM

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criticalhalt wrote:
@gibran2

I think I will try your method for recrystallization next. I had two questions:

How much water do you add to the vinegar/dirty spice solution? For example 1/2 the same or 2X the amount of vinegar.
What is in the NAOH solution? Is it just water and NAOH?

For 2-3g of DMT, I’d say 50mL of vinegar should be enough to dissolve all of it. Then add about 400-500mL additional water. No need to be exact.

To prepare your NaOH solution: add about 5g of NaOH to 100mL water.

As mumbles said, this is really just an A/B extraction. I think it’s sometimes referred to as a “mini” A/B on the forum. It’s a good way to clean up very impure spice.
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criticalhalt
#19 Posted : 9/24/2010 10:27:54 PM
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Thanks!

I have some pretty dirty stuff I've just been holding onto until I found what to do with it. The crazy part is that I don't know what I did differently from normal to mess it up in the first place. I'll read up on A/B techniques. Still slowly learning Smile

As a side note, I tried the method CrushNazT recommended and at first ended up with no crystals but just sticky yellow oil (when I started the spice was brown). I blew a fan at it overnight and when I woke up there were nice (but flat) crystals. It actually turned out pretty pure.
 
 
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