I followed the Lazyman's tek modified for 50 gram batches of Mimosa Hostilis Root Bark using bark obtained on ebay from user: xh_xavier
The ingredients used:
-500 ml of spring water
-50 grams of NaOH
-50 grams of MHRB
-unknown amount of naphtha per pull. 50 ml maybe? (non-heated)
Process:
-mixed H2O, NaOH, and MHRB together, let sit for 1-2 hours
-mixed in 1st pull of naphtha, let sit overnight or until minor emulsion settles
-pour off naphtha and evaporated under slight heat and gentle fanning
-repeat steps 2 and 3 one more time per 50 grams of MHRB
Yields:
1 - .70 grams = 1.40% yield
2 - .79 grams = 1.58% yield
3 - .92 grams = 1.84% yield
Average yield: approx 1.606%
Closing thoughts:
Logic demands an analysis of the wildly varying results. I should first note that extraction 2's yield was measured after a single recrystallization and foolish me, I forgot to weigh the initial yield.
The reason for the recrystallization was an unfortunate contamination of the product with some basic MHRB goop, though, the yield does not seem to be affected near as much as I thought a recrystallization would. Using this info, one can conservatively assume that the initial product was around .85 - .90 g's
With the second extraction assumed to be .87 g's, the new average appears to still be around 1.66%. As for the dropped yield in extraction 1, I have no explanation. All 3 extractions were preformed identically and as this is my 4th or 5th time performing the 4-5 STB extractions required for 250 g's of MHRB, I would assume learning curve does not play a role in these results.