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Voacangine from voacanga africana Options
 
Phlux-
#1 Posted : 4/25/2010 8:54:08 AM

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standard stb using dlimo as the solvent and salting with fasw - then freebased again.

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plumsmooth
#2 Posted : 4/25/2010 1:35:37 PM

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Would you be willing to outline the tek just a little bit more in detail. I'm looking for something a little stronger than Harmalas to reset my addiction receptors. Really nice looking job on that product. When you say Freebased again I imagine you evaporated then applied the same tek? That's partially where I am lost. Thanks for sharing...
 
endlessness
#3 Posted : 4/25/2010 1:49:31 PM

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I guess he mixed the dried fumarates from evaped FASW pulls with sodium carbonate, added bit of water to make paste, dried, pulled with acetone or IPA and evapped that again

nice work phlux, if you bioassay it let us know Smile
 
director of sound
#4 Posted : 7/31/2010 7:29:16 PM

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i've been doing a bit of promising research on this substance for those of us in the US that can not get ibogaine there is a rather simple procedure to reduce voacangine into ibogaine. voacangine is 16-carbomethoxy ibogaine and it is pretty easy to convert it through a saponification/hydrolysys into the wanted substance ibogaine. simply you would reflux the voacangine in 60-70% EtOH with KOH for 4-6hr and strip the ethanol off under vacuum with a hot water bath and chill the residue to 0*C and keep it there while adding 5N HCL untill a ph of 1 is obtained. you have voacangic acid now. you would warm the voacangic acid solution on a steam bath for one hour then make basic with ammonia and extract with methylene chloride and salt to your desired salt. for an HCL salt one would dissolve the ibogaine freebase in anhydrous acetone and add 30%+ HCL dropwise. the ibogaine Hcl will crystalize and precip instantly. it is especially good since out friend KT botanicals has relativly pure (stated 95%) voacangine for a good price. all other reagents used are also readily available to the average person. pure methylene chloride can be bought online at pyrotechnic hobby shops, it is used for bonding the plastic firework shells....
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