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Dark brown oil solution is all whats left??? Help please Options
 
J0rrit
#1 Posted : 3/8/2010 5:57:38 PM
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Hello,

I used this quantities: 500 ml water, 50 g mimosa, 50 g NaOH and 100 ml naphta ( x 3= 300 ml ) in total.

Now, when I put all of it in the freezer I get crystals, but they seem to be water crystals ( ice ) because when I filter them out of it they disappear. When I let all of the naphta evaporate instead of putting it in the freezer there's a dark brown substance left.... and that's all,, How can this be? Please help...

greets
 

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J0rrit
#2 Posted : 3/8/2010 8:58:24 PM
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Bump it up than... No one that has even a clu?

greets
 
stevowitz
#3 Posted : 3/8/2010 9:30:51 PM

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your crystals arent strong enough to stand the room temp filter..

freeze it again and then when you've got crystals pour the naptha into another container.
let the empty, crystal-encrusted container air dry(I use a fan) and then scrape..

for some reason room-temp naptha will melt the stuff instantly, so you gotta seperate it before drying.
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J0rrit
#4 Posted : 3/9/2010 10:49:18 AM
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I did that. I even had the container ande filter in the freezer while filtering the whole stuff.... Didn't work either. If I just let the container dry ( let all the naphta evaporate ) it should just work wright? Now it looks as if there is just no dmt in the naptha....
 
J0rrit
#5 Posted : 3/9/2010 12:32:55 PM
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Maybe it has to do with the way I separated the naptha from the rest of the substance... I had no pipet ( is that even english? Razz ) or somethng like that and I just gutted all of the naphta out in a glass ( the substance was in a coca cola bottle ) and than separated the naphta from the glass using an injection needle ( without the actual needle ) to suck out the naptha. Or does it not matter wether the naphta shakes or ruffly moves and does the dmt just be in it?

greets
 
gammagore
#6 Posted : 3/9/2010 12:37:57 PM

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The DMT should be in the naphta, I have no experience with the tek you used but sounds like you have bad bark dude.
 
 
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