Hello everyone. I was wondering if this looked correct? I am not sure, I was going to try a mini a/b. But, I was curious if this result, means I did something incorrect? I used the tek, Earth Walker posted, except I had 100g MHRB acidified with muriatic to ph3 in 500 ml distilled in a warm bath for 2.5 hrs. I then added 80 g NaCl to to 400 ml of hot water until dissolved. Followed with 500 ml of distilled water. I then added caustic soda 60 g to 300 ml of water, then into my mix. The basic solution had a pH of 13 and left it in hot water bath for 3 hrs. I added 50 ml of warm hexane then went to bed and turned off the heat. When I woke up and went to see my soup I had these sitting on top of the basic solution. I'm not sure what to do now? Do I add warm solvent and try to dissolve then pull? Also not sure if I should continue with a mini ab or not? Sorry to ask such newb questions. But, I wasn't planning on seeing the crystals already? Did I mess up by adding solvent and letting it sit so long? Thanks for any input you can give.

I’m not planning to post my response 3x…lol

If you had a plan on how to complete this project, get on with it; then come back and analyze it later.

The one place I wouldn’t have taken a break, is on the 1st pull.

Have a think about the changed variable. Then change it back. Proceed from there.

That's cool, I have never seen that before.

I'd start with the simplest and less invasive test and go from there. If i were you I'd try just heating the bottle in a hot water bath and see if the crystals dissolve back into the solvent.

I got that before and also im not chemist i can explain it and i think you did everything right but the break.

If you do a break and let it just stand for a couple of days, the dmt still travels into the solvent and cant go back, there comes a moment where the solvent is so saturated that you dont even have to freeze it to make it form crystals.
Warm the wohle thing up, let the crystals dissolve again, than do your freezing with the fullest pull you ever had. No need to worry. love is out

warm it up by a double boile and be carefull the solvent is highly flamable.
If the heating up is not enaugh to destroy the crystals, add some more solvent but not too much, so you dont loose saturation.

👍🏻

Thanks to all that replied. A little heat did wonders, thanks again!