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Not yielding enough DMT, please help! Options
 
Eluna
#1 Posted : 2/5/2010 7:13:31 AM

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Instead of evaporating try freeze precipitate.

The yellow bits were probbly dmt n-oxide
 

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geeg30
#2 Posted : 2/5/2010 3:56:23 PM

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You should try the 1g/1g/15ml ratio - MHRB/Lye/water. Naptha is based on MHRB i.e 1g/1ml

When using larger amounts of MHRB > 100g then I would use a maximum of 100ml naptha per pull - it will take more pulls but you will have a better freeze precip without having to evap some of the naptha first. Once you have rfeeze precip'd then reuse the naptha for more pulls.

You should get at least 0.5% (up to 2% with a 1% average yield) unless your bark is bunk.
Here you!!! Gonnaenodaethat

"Iceberg???? - What Iceberg????"
 
geeg30
#3 Posted : 2/6/2010 9:05:31 PM

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Nice one, Do a few more pulls (you can heat the naptha up a bit for the last one or two) and see what you get.

Enjoy
Here you!!! Gonnaenodaethat

"Iceberg???? - What Iceberg????"
 
Eluna
#4 Posted : 2/7/2010 12:51:13 PM

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nice Smile
 
geeg30
#5 Posted : 2/7/2010 4:09:38 PM

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Now use D-Limo or DCM etc to extract the jungle that remains.
Here you!!! Gonnaenodaethat

"Iceberg???? - What Iceberg????"
 
Methtical
#6 Posted : 2/8/2010 4:14:02 PM

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Everyone loves a happy ending! Smile

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shoe
#7 Posted : 2/8/2010 6:27:43 PM

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TrigZu wrote:
I did a freeze precipitation and yielded about .8 of snow. That was the third pull, I can only imagine how much I missed from the first two. The bark is not bunk! Twisted Evil


you won't have missed anything, either evapped or precipp'd, if its in the naptha, it'll come out either way. so I can't explain why it wasn't in the first two pulls, probably the base hadn't had enough time to react, especially if your bark was shredded and not powdered.

Yup, im glad you got there in the end.

Any lessons for newcommers?
shoe

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