I did a fourth pull with heptane a week after the bassifing.
Obtained a 100 of yellow spice.Didn't re.
Used a 96% etanol with 0.1%/ml benzalkonium chloride(somekinde of desinfectant) to disolve
100mg very clear criststaline hermine.It tooks some time to disolve and I used heat for it.I spreaded slowly the alcohol on 150mg of my fumable leafs until all the alcohol evaporated.
I disolved the 100 mg unrefined DMT in heptane(very little unpurity left)and spreaded the NPS on the leafs slowly untill all evaporated and let it sit for about 5 mknutes under the sun.
So at the end I had a 340mg"changa".
I did a little cigarete with about 90mg leafs smoked it in about 5 or 6 hits and didn't feel any DMT effect.The harmine effect was obvious but no DMT effect feeled.
I did a second cigarete with rest of the leafs ~250mg.Smoked it slowly and again no DMT effect feeled.So I smoked atleast an 90mg of spice and get only the harmine effect.I knlow that it could be because other alcaloides was pulled from the jar,but anyway 100mg is a lot of spice
Anyone can tell me why this happened so bad?

Did you try to smoke/vape your spice on its own to verify it is active ?
Maybe your plant material was already exhausted on the 4th pull ?

Good luck!

Probably,probably the spice wasn't active;no I didn't.But I am afraid that the reason can be this ingredient in the alcohol maybe?

Using a cigarette as the method of administration is highly inefficient, too.

And alcohol with benzalkonium chloride? Yuk!

At least get a pipe, and use clean alcohol.