So, I've been looking for a way to eliminate the water component and the boiling component of A/B & STB teks for a while now and the suggestions on this forum by some users for using ethanol looks promising (
400mg of DMT is soluble in 1mL of alcohol ). If you aren't familiar with these procedures here's some threads to read:
Extracting DMT with ethanol, vinegar and sodium carbonateIs there a way to reduce without evaporation?Acacia Extraction WorkspaceSolubility of DMT freebase in aqueous ethanol - some observationsMy questions:1) How easily will DMT move from plant material to a basic solution that is very concentrated (low water content) and the plant materiel is non-powderized & shredded? (this is in relation to
endlessness dry tek). My understanding of this extends only so far to the A/B procedure where if shredded bark is heated with water and acid, the heat will lyse the cell and the dmt will move in to the solution and react with the acid to form a salt (either dmt-hcl or dmt-acetate, etc.). This really doesn't seem to my limited understanding to be very viable with concentrated basic solutions because freebase dmt isn't soluble in water so it has no where to go, which would mean ethanol would be exceptionally handy at picking it up, if it has a solubility of
400mg of DMT in 1mL of alcohol but..
2) is sodium carbonate strong enough to open cell walls of plant material that is shredded and not powdered?(ie 2-5mm size range)3)How are you guys boiling your ethanol mixtures? (in relation to nen888 phyllode Tek Experiment 1 & 3 in the Acacia Extraction Workspace thread).
There was no talk of induction heaters in the threads linked. I read "90% ethanol with H20 will not easily catch alight (like 100% ethanol)"( nen888 ), however, from my tests of ethanol mixed with water on a gas stove with about 50ml 50/50 ethanol/water sent the pot up in flames
I'm thinking I will skip this tek and borrow a bit more from endlessness dry tek, for ease of use and also
maybe because lye is more effective at removing DMT from plant cells than combining heat and acid?...4) Are there any problems with the below method I should be aware of?After following the drytek properly and witnessing the lack of shredded bark drying, I will skip drying and simply pour basic water/ethanol solution off and dry, which after drying can then be cleaned up with anhydrous acetone (sodium carbonate insoluble in acetone) or water (freebase dmt insoluble in water). I also will experiment with other methods like
this post which involves freezing a 50/50 basified water ethanol solution and pouring it off after frozen.
My procedure is as follows:a) base shredded material with lye and minimal amount of water, enough to ensure saturation. (sodium hydroxide is used because I have assumptions that sodium carb might not be strong enough to lyse the cell walls of shredded bark).
b) skip the drying step and mix ethanol in basified bark solution
c) filter of liquid
d) mix a small amount of pure 95% ethanol in to shredded bark to remove any excess basified solution or dmt in the bark,
e) filter off and combine liquids
f) dry under a fan
g) result is freebase alkaloids + sodium hydroxide crystals
h) use multiple acetone or water washes to remove the DMT or the lye crystals.