My last reduction was a great success. After the 1st fb precipitation I re-dissolved and re-based to increase purity. And I got high yield - 6.5% post reduction.

However, after drying, it seems to be harmaline. It was THH, because in solution it didn't glow and it all crashed out under pH 10. Now it glows and feels like harmaline. I ate 400mg mix of harmine and purported THH, and was launched into 200mg harmine 200mg harmaline territory.

I'm very disappointed

I dry my THH in a heated propagator with bottom heat. I put it in a ceramic bowl and put that on the heated bottom of the prop. I keep the lid with the vents slightly open and wipe the condensation off with a cloth.

Is the prop's temperature causing the oxidation?