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A/B
Why you should weigh your DMT dose (maybe unless you're really really seasoned) Options
 
Homo Trypens
Welcoming committeeSenior Member
#1 Posted : 10/6/2021 8:18:07 PM
I did an A/B once again Smile First pull came out purrfect!

Here's a quick rundown of what i did:

- 3x 2h simmer of MHRB in ample water with a little bit of 5% acetic acid added, strained liquids into a big jar
- after cooling/settling, strained again
- reduced ~10l down to 1.5l, occasionally removing the tannin skin that formed on the surface
- strained, cooled/settled, strained again, filtered through cotton ball funnel, then coffee filter. Transferred to a 2l beaker
- based with NaOH solution. I added until it got creamy white, then black, and added a little bit more
- pulled with ~300ml of naphtha on a magnetic stirrer, with heating to 45°C
- freeze precipitated (24h), then reused naphtha for the next pull.

The first pull is the whitest i ever managed. Second and third still ok but clearly not as white.

I don't usually document my extractions anymore when there's nothing special about them, but this time i got a pic to make a point.

The left jar is second and third pulls combined. The right jar is the first pull.
Both jars contain almost exactly the same weight of DMT.
Homo Trypens attached the following image(s):
sameweightjpg.jpg (149kb) downloaded 207 time(s).
 
Voidmatrix
Welcoming committeeModerator
#2 Posted : 10/6/2021 8:40:17 PM
It's what makes scraping the dish such an exciting and surprising process. Regardless of how it looks, it's hard to tell how much is really there from one pull to the next and one extraction to the next Laughing

One love
What if the "truth" is: the "truth" is indescernible/unknowable/nonexistent? Then the closest we get is through being true to and with ourselves.


Know thyself, nothing in excess, certainty brings insanity- Delphic Maxims

DMT always has something new to show you Twisted Evil

Question everything... including questioning everything... There's so much I could be wrong about and have no idea...
All posts and supposed experiences are from an imaginary interdimensional being. This being has the proclivity and compulsion for delving in depths it shouldn't. Posts should be taken with a grain of salt. 👽
 
downwardsfromzero
ModeratorChemical expert
#3 Posted : 10/6/2021 9:39:01 PM
Good work, HT - so fluffy on the right there!

Did you record a percentage yield? And did you keep the tannin precipitates (just in case)?




“There is a way of manipulating matter and energy so as to produce what modern scientists call 'a field of force'. The field acts on the observer and puts him in a privileged position vis-à-vis the universe. From this position he has access to the realities which are ordinarily hidden from us by time and space, matter and energy. This is what we call the Great Work."
― Jacques Bergier, quoting Fulcanelli
 
shroombee
#4 Posted : 10/7/2021 1:43:42 AM
Great photo! This should be a meme "Why weigh your DMT? These jars contain the same weight of DMT. Any questions?"
 
Voidmatrix
Welcoming committeeModerator
#5 Posted : 10/7/2021 2:29:39 AM
shroombee wrote:
Great photo! This should be a meme "Why weigh your DMT? These jars contain the same weight of DMT. Any questions?"


Just makes me think about the number of eye rolls I've given to people that don't understand why I double check my doses Laughing

One love
What if the "truth" is: the "truth" is indescernible/unknowable/nonexistent? Then the closest we get is through being true to and with ourselves.


Know thyself, nothing in excess, certainty brings insanity- Delphic Maxims

DMT always has something new to show you Twisted Evil

Question everything... including questioning everything... There's so much I could be wrong about and have no idea...
All posts and supposed experiences are from an imaginary interdimensional being. This being has the proclivity and compulsion for delving in depths it shouldn't. Posts should be taken with a grain of salt. 👽
 
null24
Welcoming committeeModerator
#6 Posted : 10/7/2021 3:46:34 AM
That's the fluffiest public service announcement I've ever seen!Thumbs up
Sine experientia nihil sufficienter sciri potest -Roger Bacon
*γνῶθι σεαυτόν*
 
Homo Trypens
Welcoming committeeSenior Member
#7 Posted : 10/8/2021 2:22:49 PM
Hehe, thanks all of you Smile

downwardsfromzero wrote:
Did you record a percentage yield? And did you keep the tannin precipitates (just in case)?


Yes and yes Smile Currently, i recovered 0.7%.

I think i reduced too much, i'm still pulling (5th now, still some coming).
The spent bark and all the sludges are sitting in a jar, based, waiting to be pulled when i'm done with the soup.

4th and 5th pulls are back to white and fluffy btw! I hadn't cleaned the dish for 2nd and third, thought the scrape residue would help form nicer crystals. For 4th and 5th i washed the dish with IPA (that i collect in another jar of course), and there were white blobs again.
 
Tony6Strings
#8 Posted : 10/8/2021 6:10:39 PM
I have also noticed the tendency of white fluffy crystal to appear as a much larger pile than other textures (powdery dmt, waxes, goo or denser crystal). It is a mindf*ck to scoop out your usual sized knifetip onto the scale and it weighs only a fraction of what the same knifetip usually does.

Nice work cool jars.
olympus mon wrote:
You need to hit it with intention to get where you want to be!

"Good and evil lay side by side as electric love penetrates the sky..." -Hendrix

"We have arrived at truth, and now we find truth is a mystery- a play of joy, creation, and energy. This is source. This is the mystic touchstone that heals and renews. This is the beginning again. This is entheogenic." -Nicholas Sand
 
 
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