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mass spec update Options
 
benzyme
Moderator | Skills: Analytical equipment, Chemical master expertExtreme Chemical expert | Skills: Analytical equipment, Chemical master expertChemical expert | Skills: Analytical equipment, Chemical master expertSenior Member | Skills: Analytical equipment, Chemical master expert
#1 Posted : 11/30/2018 10:09:14 PM
It's not like me to ask for help, but I'm a bit down on my luck. MS is down, FTIR has a bad motherboard, and UV detector is down too (bad motherboard as well). I'll focus on LC-MS...the mass spec has a bad power supply, and a new one isn't cheap.
Wife's father just died on thanksgiving, and we're going to support her mother (her siblings will pitch in too), so money is a bit tight.

Those who know me, know I am dedicated to the art of analysis, and for those that donate, I will run free analyses until March, once I get back up and running. Aside from the power supply, the turbopump is still kickin', and the UHPLC pump is operational. I pretty much only do analysis for the Nexus, it is home. I'm the sole proprietor, so my reputation is everything.

Donations can be made to my XMR or BTC accounts in my sig, or benmartineziii@gmail.com on paypal.
"Nothing is true, everything is permitted." ~ hassan i sabbah
"Experiments are the only means of attaining knowledge at our disposal. The rest is poetry, imagination." -Max Planck
 
benzyme
Moderator | Skills: Analytical equipment, Chemical master expertExtreme Chemical expert | Skills: Analytical equipment, Chemical master expertChemical expert | Skills: Analytical equipment, Chemical master expertSenior Member | Skills: Analytical equipment, Chemical master expert
#2 Posted : 11/30/2018 11:44:20 PM
thanks for the ETH Pleased
every little bit helps.

There are some neat projects in the pipeline, like melatonin-doped mushies, melatonin to 5-MeO conversion, tryptophan to hyperspace, and 20 mM tryptamine-doped cubes. It's going to be an interesting winter Big grin
"Nothing is true, everything is permitted." ~ hassan i sabbah
"Experiments are the only means of attaining knowledge at our disposal. The rest is poetry, imagination." -Max Planck
 
Mindlusion
Extreme Chemical expertChemical expertSenior Member
#3 Posted : 12/1/2018 2:21:18 AM
Sorry to hear the news benz, I hope your winter gets brighter from here on out. (It will technically after Dec. 21st)
Expect nothing, Receive everything.
"Experiment and extrapolation is the only means the organic chemists (humans) currrently have - in contrast to "God" (and possibly R. B. Woodward). "
He alone sees truly who sees the Absolute the same in every creature...seeing the same Absolute everywhere, he does not harm himself or others. - The Bhagavad Gita
"The most beautiful thing we can experience, is the mysterious. The source of all true art and science."
 
Loveall
Chemical expertSenior Member
#4 Posted : 12/5/2018 9:05:53 PM
Bump, this is important work for our community. Good luck benzyme!
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benzyme
Moderator | Skills: Analytical equipment, Chemical master expertExtreme Chemical expert | Skills: Analytical equipment, Chemical master expertChemical expert | Skills: Analytical equipment, Chemical master expertSenior Member | Skills: Analytical equipment, Chemical master expert
#5 Posted : 12/5/2018 9:52:56 PM
Thanks so much, that certainly expedites things.
Hopefully by next friday, either the PS will be repaired, or I’ll just order a new one.
"Nothing is true, everything is permitted." ~ hassan i sabbah
"Experiments are the only means of attaining knowledge at our disposal. The rest is poetry, imagination." -Max Planck
 
benzyme
Moderator | Skills: Analytical equipment, Chemical master expertExtreme Chemical expert | Skills: Analytical equipment, Chemical master expertChemical expert | Skills: Analytical equipment, Chemical master expertSenior Member | Skills: Analytical equipment, Chemical master expert
#6 Posted : 12/6/2018 2:51:00 PM
I ordered it.
Wifey said to just go ahead and buy it, with monies from savings, so I covered the difference.
Thank you kindly to those who pitched in, it really means alot to me.
I should have it by next week, Thermo has to ship it to my work address.

I’ll update when it is up and running, so I can start accepting samples for testing.
"Nothing is true, everything is permitted." ~ hassan i sabbah
"Experiments are the only means of attaining knowledge at our disposal. The rest is poetry, imagination." -Max Planck
 
Loveall
Chemical expertSenior Member
#7 Posted : 12/6/2018 5:00:23 PM
Great news, deep thanks Benzyme.

I'm really wondering what this green-fluorescent flaky stuff is from a mushroom extract. Bad news is that I'm struggling to reproduce it, maybe because proteins are tricky.
Loveall attached the following image(s):
IMG_20181206_115506543.jpg (3,163kb) downloaded 298 time(s).
IMG_20181206_115730921.jpg (1,850kb) downloaded 298 time(s).
💚🌵💚 Mescaline CIELO TEK 💚🌵💚
💚🌳💚DMT salt e-juice HIELO TEK💚🌳💚
💚🍃💚 Salvinorin Chilled Acetone with IPA and Naphtha re-X TEK💚🍃💚
 
benzyme
Moderator | Skills: Analytical equipment, Chemical master expertExtreme Chemical expert | Skills: Analytical equipment, Chemical master expertChemical expert | Skills: Analytical equipment, Chemical master expertSenior Member | Skills: Analytical equipment, Chemical master expert
#8 Posted : 12/8/2018 5:14:22 AM
Shouts out to Loveall, ducdevil, and Sunnyside. You guys will get priority free analysis.
I was very bummed out, but your generosity motivated me to get back up. I have to keep doin' what I do, it's greater than myself. Thank you so much.
"Nothing is true, everything is permitted." ~ hassan i sabbah
"Experiments are the only means of attaining knowledge at our disposal. The rest is poetry, imagination." -Max Planck
 
benzyme
Moderator | Skills: Analytical equipment, Chemical master expertExtreme Chemical expert | Skills: Analytical equipment, Chemical master expertChemical expert | Skills: Analytical equipment, Chemical master expertSenior Member | Skills: Analytical equipment, Chemical master expert
#9 Posted : 12/8/2018 4:03:30 PM
during better days:

https://vimeo.com/293620635

"Nothing is true, everything is permitted." ~ hassan i sabbah
"Experiments are the only means of attaining knowledge at our disposal. The rest is poetry, imagination." -Max Planck
 
benzyme
Moderator | Skills: Analytical equipment, Chemical master expertExtreme Chemical expert | Skills: Analytical equipment, Chemical master expertChemical expert | Skills: Analytical equipment, Chemical master expertSenior Member | Skills: Analytical equipment, Chemical master expert
#10 Posted : 12/10/2018 4:21:23 AM
lobo and pinkoyd..thank you, guys. Thumbs up
hopefully it arrives to work this week. Of course, I'll keep y'all posted.
"Nothing is true, everything is permitted." ~ hassan i sabbah
"Experiments are the only means of attaining knowledge at our disposal. The rest is poetry, imagination." -Max Planck
 
benzyme
Moderator | Skills: Analytical equipment, Chemical master expertExtreme Chemical expert | Skills: Analytical equipment, Chemical master expertChemical expert | Skills: Analytical equipment, Chemical master expertSenior Member | Skills: Analytical equipment, Chemical master expert
#11 Posted : 12/11/2018 3:38:42 PM
aaargh! Crying or very sad

I called Thermo, they told me that it's backordered, anticipated ship date Feb. 20. The lady is going to email me back
with other sourcing/shipping options. Gonna email the guy who's repairing my faulty PS. this is frustrating
"Nothing is true, everything is permitted." ~ hassan i sabbah
"Experiments are the only means of attaining knowledge at our disposal. The rest is poetry, imagination." -Max Planck
 
benzyme
Moderator | Skills: Analytical equipment, Chemical master expertExtreme Chemical expert | Skills: Analytical equipment, Chemical master expertChemical expert | Skills: Analytical equipment, Chemical master expertSenior Member | Skills: Analytical equipment, Chemical master expert
#12 Posted : 12/13/2018 4:49:37 PM
ok..
the guy repairing it called me this morning, he ordered a capacitor and an IC, and should have it done by monday.
"Nothing is true, everything is permitted." ~ hassan i sabbah
"Experiments are the only means of attaining knowledge at our disposal. The rest is poetry, imagination." -Max Planck
 
ducdevil
#13 Posted : 12/13/2018 5:21:36 PM
YAY! Big grin
That's the holiday spirit...
 
benzyme
Moderator | Skills: Analytical equipment, Chemical master expertExtreme Chemical expert | Skills: Analytical equipment, Chemical master expertChemical expert | Skills: Analytical equipment, Chemical master expertSenior Member | Skills: Analytical equipment, Chemical master expert
#14 Posted : 12/18/2018 3:13:05 AM
Crying or very sad

the repair was unsuccessful. I put in the order for the part.
*sighs*
"Nothing is true, everything is permitted." ~ hassan i sabbah
"Experiments are the only means of attaining knowledge at our disposal. The rest is poetry, imagination." -Max Planck
 
Loveall
Chemical expertSenior Member
#15 Posted : 12/18/2018 3:54:18 AM
Thanks for all your efforts benzyme. So ETA for the part is still ~ Feb 20, right?
💚🌵💚 Mescaline CIELO TEK 💚🌵💚
💚🌳💚DMT salt e-juice HIELO TEK💚🌳💚
💚🍃💚 Salvinorin Chilled Acetone with IPA and Naphtha re-X TEK💚🍃💚
 
benzyme
Moderator | Skills: Analytical equipment, Chemical master expertExtreme Chemical expert | Skills: Analytical equipment, Chemical master expertChemical expert | Skills: Analytical equipment, Chemical master expertSenior Member | Skills: Analytical equipment, Chemical master expert
#16 Posted : 12/18/2018 3:55:47 AM
correct. 2/21 was what was quoted via email.
"Nothing is true, everything is permitted." ~ hassan i sabbah
"Experiments are the only means of attaining knowledge at our disposal. The rest is poetry, imagination." -Max Planck
 
endlessness
Moderator
#17 Posted : 12/18/2018 10:59:04 AM
Benz, glad to hear at least things are going in the right direction!

Thanks to all who donated to benz!

Same for EC's equipment, finally we got a word from the main donor that he will pay for the LC-MS yearly maintenance, so we should have it up and running again early next year Smile
 
benzyme
Moderator | Skills: Analytical equipment, Chemical master expertExtreme Chemical expert | Skills: Analytical equipment, Chemical master expertChemical expert | Skills: Analytical equipment, Chemical master expertSenior Member | Skills: Analytical equipment, Chemical master expert
#18 Posted : 12/20/2018 2:59:45 AM
I put in a cancel email, I'm not sure it is a compatible PS.
but this one is, so I put in an offer for $1501. It is both the +36 V/-28 V switching, and a 200 V linear PS below it (just in case that one is bad too). Two power supplies for the price of one.
"Nothing is true, everything is permitted." ~ hassan i sabbah
"Experiments are the only means of attaining knowledge at our disposal. The rest is poetry, imagination." -Max Planck
 
benzyme
Moderator | Skills: Analytical equipment, Chemical master expertExtreme Chemical expert | Skills: Analytical equipment, Chemical master expertChemical expert | Skills: Analytical equipment, Chemical master expertSenior Member | Skills: Analytical equipment, Chemical master expert
#19 Posted : 12/20/2018 2:19:11 PM
offer accepted, paid.
"Nothing is true, everything is permitted." ~ hassan i sabbah
"Experiments are the only means of attaining knowledge at our disposal. The rest is poetry, imagination." -Max Planck
 
benzyme
Moderator | Skills: Analytical equipment, Chemical master expertExtreme Chemical expert | Skills: Analytical equipment, Chemical master expertChemical expert | Skills: Analytical equipment, Chemical master expertSenior Member | Skills: Analytical equipment, Chemical master expert
#20 Posted : 12/27/2018 12:06:41 AM
Crying or very sad

It didn't work. There must be a short somewhere. *sighs*
I'm not electrically inclined, and even if I were, Thermo will not provide schematics. I have neither the time nor money
to pursue this at the moment, so I initiated a return, and will refund everyone who donated. This sucks, I'm sorry.
"Nothing is true, everything is permitted." ~ hassan i sabbah
"Experiments are the only means of attaining knowledge at our disposal. The rest is poetry, imagination." -Max Planck
 
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