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Saturated Naptha is now mixed in water. HELP! Options
 
Hazey82
#1 Posted : 2/10/2015 2:26:00 AM
I wanted to recrystallize some product that was of a dark tan color, so I heated up some Naphtha (150ml) in a glass using a double boil and added the spice and continued heating and mixing to further dissolve. The glass cracked and naptha has mixed in with the boiling water in the pot.

I transferred the water now containing the spice and Naptha into a bottle and thought I could just add some acid PH 2.5 and I would be able to do a mini A/B but it is not separating.
This is how it looks, can someone advise how I can save this please.

 
SynKyd
#2 Posted : 2/10/2015 4:14:32 AM
Basify that solution for the naphtha to separate.Thumbs up
At the center of this existence, it is everything and nothing, all of us and each of us and none of us. My light is now lit, and it cannot be extinguished.
 
Hazey82
#3 Posted : 2/10/2015 4:19:28 AM
SinysterKyd wrote:
Basify that solution for the naphtha to separate.Thumbs up

Cheers, I was thinking that but wanted to be sure.
I assume aiming for a PH of around 12+, then just shake around and let separate a few times? There is about 150-200ml of naptha in there will all of the molecule get carried over ?
 
The Day Tripper
#4 Posted : 2/10/2015 7:51:48 PM
Hazey82 wrote:
SinysterKyd wrote:
Basify that solution for the naphtha to separate.Thumbs up

Cheers, I was thinking that but wanted to be sure.
I assume aiming for a PH of around 12+, then just shake around and let separate a few times? There is about 150-200ml of naptha in there will all of the molecule get carried over ?


How much dmt do you think was in your starting product?

I'd just base it, put it in a more narrow neck container to ease siphoning off, or use a sep funnel if you have one, and do 3 pulls/freezes with your naptha.

That should assure most of your dmt gets recovered from the water.
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