Hello again

ok, back to questions

previously i ask about time need to growing to collect 1kg.
Anticipating questions why that much, i think 10g dmt for 1-2 year its not nothing "Big"
but anyway. How long can take growing to get that amount of powder?

and second one, in Polnad nobody use naphtha to extract.
We use heptane/hexen.

Which method is better? what's the difference

There are best know method using in Poland.

1. grind bark dust.
2. You put the bark to pot
3. inundated with water to a level slightly below the bead, so as not seethed
4. The water acidified with citric acid to pH = 3 (or 4, or even 0 - so far as it acidic, but discourage pouring cock a lot of acid - tablespoon flat enough, pouring the much later result in the need to use large amounts of sodium hydroxide)
5. you cook on low heat for up to 2 hours of boiling
6. Drain the tea, be filtered it through attrition and accrue in another bowl.
7. You repeat steps 2-6 again
8. The acid extracts were collected (should be near the fluid 6-7l) inserting a few large pots in order to reduce the volume to 1400 ml / kg used cortex
9. Waiting until the solution becomes reduced and sieve the cold again through coffee filters. At this stage have a mass concentration of compounds contained in plants and the alkaloids, including DMT, in the form of a salt of tartaric acid.
10. The solution is poured into a separatory funnel or a minimum of 2 liter, glass, narrow vessels and adjusted to pH = 12-14 with NaOH - Carefully pour granules - at the same time not more than 20g, after every pour vigorously - will be intensively warmed - be before the next portion of the solution cool down rules DMT otherwise be destroyed. After this process, tartaric acid residue DMT tartrate molecules are reacted with a sodium releasing DMT molecule to the free base (freebase). It is necessary to obtain crystals.
11. The warm alkaline solution pour 200 ml hot hexane / heptane / - stirred vigorously and after 5 minutes of non-polar layer was separated, saturated free base N, N-dimethyltryptamine. NOTE: If you do need to strongly heat the emulsion distributor and sprinkle solid NaCl - if it does not help that chapel. The emulsions are not formed at very DOKLADIE filtered solution (ideally used for this purpose G4 fritted funnel), and therefore filtration steps in the previous steps are essential. The extraction was repeated three times using fresh solvent.
12. You collect non-polar extracts, pour into a glass bowl and top covers the aluminum-foil tightly and then allowed to stand in the freezer for 3 days.
13. After 3 days the solvent You blend carefully - on the walls of the entire DMT crystallized in hexane in the form of snow-white crystals.

Hey,

Regarding the growing, I don't really think its a plausible way of collecting bark according to what I have seen on this forum.

Hexane and heptane can be used as NPS, heptane is also a specifically good solvent for recrystallisation too. I think hexane is generally more selective than naptha which is a mix of various hydrocarbons. Naptha is generally cheaper, check the wiki for info on hexane as a solvent there is some good information there.

You might want to try this tek - Cyb's Tek

Never stir the basic solution 'vigorously' when the NPS is added, this can cause emulsions to form. Also, I don't think the DMT would be 'destroyed' by not allowing the solution to cool when adding NaOH.