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defatting and jungle spice? Options
 
decibel
#1 Posted : 6/9/2014 4:08:35 PM
Hi there fellow nexians Smile

I'm about to prepare for my second extraction and have been reading a lot of wisdom since my first extraction, which was a big mess Razz I did an A/B extraction from the DMT Handbook tek, using MHRB instead of Acacia Obtusifolia which they use in the DMT Handbook. My end result was a big pile of black brown gunk with yellow gunk underneath! I cleaned it up with some hot water with NaOH and Naptha and siphoned the layers much more carefully, and got this yellowish flake-like spice, which was absolutely awesome! Big grin Then I bought some separatory funnels, purified my spice, till it was as white as the purest snow and as dull as it was white Surprised

Lately I have read Entropymancer's posts about extractions and Jungle Spice which I am pretty confident was what I got from my first extraction. So my questions are:


- If I want to be sure of getting jungle spice should I skip the defatting step in extractions. And maybe even go and make an STB extraction instead of an A/B extraction?

- I did get this beautiful result the first time with an A/B extraction, but was this a lucky consequence from my first-time-sloppiness? Is it always a good idea to acidcook - does it ensures me a bigger yield? Or should I avoid it if I want to get this other alkoloids?

- Also, are there other impurities that I should be aware of that can cause same colorization? And maybe some tips to how I can tell them apart? (if such a thing is possible without professional equipment)

- And at last I'd like to know if NaOH and lye are the same thing? If not: Are Sodium Carbonate washes always important or only when using lye?
 
highRvibratoryfreq
#2 Posted : 6/9/2014 6:41:22 PM
i would suggest acid cooking > reducing > base > then pulling with xylene/limonene > and salting with more acetic acid > then converting with sodium carbonate and pulling with acetone. this should yield a nice coloured full spectrum junglespice.
 
decibel
#3 Posted : 6/10/2014 1:48:44 PM
highRvibratoryfreq wrote:
i would suggest acid cooking > reducing > base > then pulling with xylene/limonene > and salting with more acetic acid > then converting with sodium carbonate and pulling with acetone. this should yield a nice coloured full spectrum junglespice.

At the point where I'll be salting with more acetic acid - would this be the xylene/limonene I would be salting?
Which I then would add sodium carbonate and acetone, then separate and precipitate?
 
 
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