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Fumarate to Freebase Conversion Problem- Need Help!! Options
 
J_Mags82
#1 Posted : 4/27/2014 3:33:05 PM
Hello, my name is Jeremy. This is my first post since becoming a Nexus member.

Im not completely new to dmt extractions, so far ive been able to produce some clean white dmt, using a basic STB tek. Then turning it into changa. But in my attempts to extract the jungle dmt afterwards, Ive run into some issues, and i would really appreciate any help in figuring out what the problem is..

I started with about 500 grams MHRB in two large jars, I did several naphtha pulls, extracting most of the white dmt. Then i began pulling for jungle using d-limonene, did 3x pulls. The saturated d-limo came out cloudy so i put in the freezer several times, letting some of the solids settle, and decanting each time. Once my d-limo became clear enough, I salted out the fumarate using FASI (Fumaric Acid Saturated IPA). I did this slowly and correctly. But once i recovered my fumarate, it didnt look like any other ive seen online. It was a very thick red goo, which ive read is common, but when scraped up and let completely dry, it turned into hard little 'dirt rocks' ??? My first question is if this is common, if the fumarate is good as is or if its extremely impure?

At this point, i wasnt sure how impure the fumarate was, so i did a cold IPA wash to clean it up a bit. After, i began to try to convert fumarate to freebase. But when dissolving the fumarate into water, the water became very cloudy, as if adding dirt to water. This is also unlike any pics ive seen online, which shows the water being clear. I let the fumarate/water settle out some of the solids, i decanted and began to freebase using saturated sodium carbonated water, but the fumarate water was still pretty cloudy. Now im waiting to see if any crystals will precipitate in the cloudy solution.. So basically im just wondering if everything is looking good, or if my fumarate is very impure or if something else went wrong??

Im adding pics of my fumurate after being scraped and of how it looks once dissolved into water and a pic of the fumarate/water shown in the BLAB tek. If anyone can reply with any insight i would be really thankful..

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200px-Dissolvedfumarate.jpg (11kb) downloaded 32 time(s).
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