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Question on an unidentified solvent Options
 
Attention All Shipping
#1 Posted : 6/23/2009 4:22:11 PM
I’ve mentioned previously on another thread that I had had problems with an extraction using heptane. It turned out that despite being sold as such the heptane wasn’t heptane as nothing freeze precipitated from it but adding FASA did result in something precipitating out. I’ve now pulled some MHRB with it (after pulling with Bartoline naphta) and evaporated it to yield a small quantity of yellow waxy sticky product, the effects of which are quite pleasant and described here

What I want to ask if if anyone can help identify the solvent, which I’ve been calling non-heptane. I know it is more non-polar than heptane, works with FASA, doesn’t freeze precipitate spice, isn’t Toluene or Xylene (as it doesn’t evaporate in their distinctive spotty patterns but as a white coating on the evap dish which scrapes up yellow), is clear in colour & smells the same as any other hydrocarbon solvent. I’ll add a pic of the extracted product incase anyone’s yielded similar but I won’t be able to do this for a while as I’m waiting for a new computer & can’t post pics from my work pc. Still if you’ve yielded a similar mellow yellow product with similar effects let me know what solvent you used as I’m really interested in indentifying this non-heptane.
 
benzyme
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#2 Posted : 6/23/2009 8:44:26 PM
would you happen to know its boiling point?
if it glows significantly in a black light, it's an aromatic hydrocarbon solvent (like toluene or xlyene). it won't glow if it's heptane (an aliphatic, straight-chain hydrocarbon)
"Nothing is true, everything is permitted." ~ hassan i sabbah
"Experiments are the only means of attaining knowledge at our disposal. The rest is poetry, imagination." -Max Planck
 
Attention All Shipping
#3 Posted : 6/24/2009 1:03:35 PM
I'll check this out tonight.
 
Attention All Shipping
#4 Posted : 6/25/2009 1:05:10 PM
It starts boiling at 84 degrees centigrade.
There is a purple flourescence when a UV torch is shone through it i the dark.
 
benzyme
Moderator | Skills: Analytical equipment, Chemical master expertExtreme Chemical expert | Skills: Analytical equipment, Chemical master expertChemical expert | Skills: Analytical equipment, Chemical master expertSenior Member | Skills: Analytical equipment, Chemical master expert
#5 Posted : 6/25/2009 7:28:04 PM
hmm..sounds like some sort of aliphatic, although aliphatics don't really fluoresce unless unsaturated (has alternating double bonds)

aromatics start boiling at 80.1 (benzene), but glow brightly (blue). benzene has a distinctly sweet smell, as does toluene. xylene smells annoying
"Nothing is true, everything is permitted." ~ hassan i sabbah
"Experiments are the only means of attaining knowledge at our disposal. The rest is poetry, imagination." -Max Planck
 
 
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