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is my bark still any good? Options
 
BoDigga420
#1 Posted : 1/21/2014 10:10:56 PM
Hey everybody, this is my first time posting here. I just attempted my first extraction, an a/b of acacia confusa. I had 500 grams boiling in 2000ml of water with 100ml of phosphoric acid over an electric stovetop. I foolishly left its side for about an hour, and when I came back all of the water had evaporated and the bark was smoking. i quickly added another liter of water to the pot, but i'm afraid that the damage has already been done. Do you think the bark is salvageable or has all the dmt been burnt up?
 
BoDigga420
#2 Posted : 1/21/2014 10:16:17 PM
if anyone takes the time to read this, thank you so much. i forgot to mention that in original post
 
Professor Paradise
#3 Posted : 1/21/2014 10:40:03 PM
Too much heat can damage sensitive compounds.

If it isn't burnt I would still proceed with the extraction, though your yield may not be as good.
 
BoDigga420
#4 Posted : 1/21/2014 10:46:20 PM
some of the bark was obviously destroyed as it was blackened and crispy but Im going to go on and cross my fingers. I'll post yield (if any) when I'm finished
 
Professor Paradise
#5 Posted : 1/21/2014 11:32:28 PM
I hope you don't end up with burnt compounds in your extract.

Good luck!
 
Warrior
#6 Posted : 1/22/2014 12:32:53 AM
You should still be able to do the extraction just fine. It may affect the crystals, but active compound is active compound. Maybe someone more familiar with the combustion products of the actives can chime in, but the products are most likely inert (hopefully).
 
BoDigga420
#7 Posted : 1/22/2014 1:05:43 AM
Thanks everyone! Very happy
I'm hoping only the bottom of the bark was burnt, I have to imagine that it couldn't have been burning for long as it was only about an hour from when I put it on the stove. most of it is still a nice red color as it should be
 
Mister_Niles
#8 Posted : 1/22/2014 1:50:37 AM
An unwatched pot..... catches on fire! I hope you learned from this experience, or you'll never cook a good risotto Smile
Welcome Home Mister_Niles. We've Been Waiting For You.


"Don't worry. When it happens, you won't be able to not let it do its thing. You won't have the ability to distinguish a pen from a hippopotamus"
- Art Van D'lay
 
indydude19
#9 Posted : 1/22/2014 2:36:30 AM
Were you able to tell if it was the bark smoking or just the last parts of solution boiling off?

I recently did an extraction where I did the same careless thing but I caught it in time to where the bark was still saturated and unburned. Just the last free reservoirs of solution were boiling away (though a negligible amount of bark burnt to the pot on the stoves hot spots).

I continued through the extraction and am currently seeing the beginnings on what I anticipate to be a nice yield based on the current formation and how freakishly cloudy the naphtha is on the first pull.
I died a mineral, and became a plant. I died a plant and rose an animal. I died an animal and I became human. Then why fear disappearance through death? Next time I shall die, Bring forth wings and feathers like angels; After that, soaring higher than angels-- What you cannot imagine, I shall be that.

Any speakings written are the purely fictional ramblings of an illiterate grande taco, and are false in the face of truth when judged by the all-father. They are in no way real.
 
BoDigga420
#10 Posted : 1/28/2014 5:45:41 PM
indydude, the bark was definately smoking. the room was full of smoke that had a different smell to the acacia steam.

well, I did a pull and evaporated it due to lack of a cold freezer, and as I had feared the product is inactive Sad
 
Warrior
#11 Posted : 1/28/2014 6:34:50 PM
Uhhh... You need a freezer to precipitate the final product. What were you planning to do without a freezer?

I would recommend planning better next time. It sounds like there were multiple things that went wrong but could have been avoided.
 
Entheogenerator
#12 Posted : 1/28/2014 7:07:27 PM
Warrior wrote:
Uhhh... You need a freezer to precipitate the final product. What were you planning to do without a freezer?

I would recommend planning better next time. It sounds like there were multiple things that went wrong but could have been avoided.

Uhhh... Evaporation works every bit as well, although perhaps leaving a slightly more impure product... Evaporation was standard procedure in the days before freeze-precipitation. Please doing some additional research before taking a condescending tone with newcomers.

BoDigga420, I'm sorry to hear about the results. Unfortunately, one can expect to waste a little bit of bark in the process of learning hwo to extract. Next time, I would suggest starting with small batches of 100g or so. This way if something goes wrong, you've only wasted 100g; and working through 500g bark would give you the experience of 5 extractions rather than only one. Practice makes perfect! Smile
"It's all fun and games until someone loses an I" - Ringworm
Attitude PageHealth & SafetyFAQKnown Substance InteractionsExtraction TeksThe Machine

 
BoDigga420
#13 Posted : 1/29/2014 7:55:57 AM
Warrior wrote:
Uhhh... You need a freezer to precipitate the final product. What were you planning to do without a freezer?

I would recommend planning better next time. It sounds like there were multiple things that went wrong but could have been avoided.


You are absolutely correct. I made several foolish mistakes such as not watching the soup that could have prevented this from happening, but whats done is done. Now at least I am more comfortable with the procedure and the next extraction can go smoothly.

Entheogenerator, Im definitely going to take your advice next time. Thanks so much Smile
 
Warrior
#14 Posted : 1/29/2014 8:19:29 PM
Entheogenerator wrote:

Uhhh... Evaporation works every bit as well, although perhaps leaving a slightly more impure product... Evaporation was standard procedure in the days before freeze-precipitation. Please doing some additional research before taking a condescending tone with newcomers.


Precipitate. Not evaporate.
 
Warrior
#15 Posted : 1/29/2014 8:23:52 PM
BoDigga420 wrote:

You are absolutely correct. I made several foolish mistakes such as not watching the soup that could have prevented this from happening, but whats done is done. Now at least I am more comfortable with the procedure and the next extraction can go smoothly.
[...]


Yeah, we learn from trial and error. The important part is to learn from everything you try, and to develop skill of execution.

Best wishes to you!
 
Entheogenerator
#16 Posted : 1/29/2014 10:47:06 PM
Warrior wrote:
Precipitate. Not evaporate.

Right, but BoDigga420 didn't say anything about precipitation. Your post implied there was no alternative to freeze-precipitation.
"It's all fun and games until someone loses an I" - Ringworm
Attitude PageHealth & SafetyFAQKnown Substance InteractionsExtraction TeksThe Machine

 
TryptamineChampion
#17 Posted : 1/29/2014 10:54:04 PM
BoDigga420 wrote:
Hey everybody, this is my first time posting here. I just attempted my first extraction, an a/b of acacia confusa. I had 500 grams boiling in 2000ml of water with 100ml of phosphoric acid over an electric stovetop. I foolishly left its side for about an hour, and when I came back all of the water had evaporated and the bark was smoking. i quickly added another liter of water to the pot, but i'm afraid that the damage has already been done. Do you think the bark is salvageable or has all the dmt been burnt up?


Y Not Try The Noman Tek? The Heat Is Gonna Destroy Everything
 
Entheogenerator
#18 Posted : 1/30/2014 6:14:22 AM
TryptamineChampion wrote:
Y Not Try The Noman Tek? The Heat Is Gonna Destroy Everything

Heat will not destroy everything. Too much heat will break down the active alkaloids, but the right amount of heat will make an extraction much more thorough and efficient than it would be if it had been done at room temperature.

A/B extractions are also far more efficient than STB extractions like Noman's. In addition: many people, including myself, have tried STB extractions on Acacia confusa without having good results.
"It's all fun and games until someone loses an I" - Ringworm
Attitude PageHealth & SafetyFAQKnown Substance InteractionsExtraction TeksThe Machine

 
halfhead
#19 Posted : 1/30/2014 6:38:09 AM
This is a great question, I have almost done this... a couple times... so knowing if the next 8 hours is worth my time would be great information!

A question I would like to add is, if you are drawing the salt(dmt) from the bark to the acidified water, and you boil off all the water, does the salt stay in the mix or evaporate out?
If it DOES boil/evaporate out, then depending on bark quantity and time spent boiling, could give you an idea of how much dmt is lost, i would assume.
Open source consciousness... The way it should be!

-hH
 
3rdI
#20 Posted : 1/30/2014 9:03:34 AM
the Magic wont evap at water boiling temps, if it did you wouldn't be able to reduce Aya brews.
INHALE, SURVIVE, ADAPT

it's all in your mind, but what's your mind???

fool of the year

 
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