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Extracting from Desmodium pulchellum Options
 
dzznutzz
#1 Posted : 11/7/2013 2:55:46 PM
hi guys ,
ive noticed this plant while looking at trouts notes on the demodium genus... whole plant is active with different alkaloid makeup in different parts of the plant... lucky for me this is abundant in the north east thailand ... so far i have extracted from 300g leaf using blab tek... pulling with d-limonene(room temp) and then xylene/naphtha mix.. Pulls then salted out using vinegar... the main reason i wanted to post this is extraction is because each pull salted out a different product... really would like peoples opinion on what i have here and what my options are Smile

First 3 photos are d-limonene pulls salted with vinegar evaporated at room temp
Last 2 were pulled later using a naphtha/xylene mix (80/20) salted with vinegar

trouts notes states the following ...
Mature stem and leaf (1.4% Total alkaloid)
Gramine - 0.098%
N,N-DMT - 0.294%
DMT-N-oxide - 0.070%
5-Hydroxy-N-methyltryptamine - 0.056%
Bufotenine - 0.112%
Bufotenine-N-oxide - trace
5-Methoxy-N-methyltryptamine - 0.154%
5-Methoxy-DMT - 0.476%
5-Methoxy-DMT-N-oxide - 0.070%
6-Methoxy-Nb-methyl- H4-β-carboline - 0.028%
Unidentified bases


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