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necessary time for freeze-precipitation? Options
 
NeuroExplorer
#1 Posted : 10/17/2013 2:07:42 AM
Hi All,

Using the protocol from "The DMT handbook"; I was wondering if it is necessary to freeze precipitate for 72 hours, when after 48 hours i already have what appears to be quite a substantial yeald of spice?

What does everyone else recommend?

Also, can anyone forsee any issues with leaving this in the freezer for an extended period (such as 1 week)?

Cheers!
 
arcologist
#2 Posted : 10/17/2013 3:36:51 AM
I find that 12 hours is usually sufficient. A good rule of thumb is to wait until the naphtha becomes totally transparent (not cloudy). At this point, all of the DMT that would precipitate already has.
 
DreaMTripper
#3 Posted : 10/17/2013 3:41:14 AM
The longer the better but undisturbed for 3 whole days is ideal, 2 is ok too.
Just reuse for the next pull and after the last pull leave it for 5 days solid decant from spice and evaporate to recover any left, if there is any.
 
The Day Tripper
#4 Posted : 10/17/2013 3:48:58 AM
It matters not, just take the solvent and pour it off, evaporate it a bit, and pour it back in.

Repeat until theres very little left, or none at all depending on how carefully you seperated your solvent and basic water phases.

Thats what i do

Good to the last drop Laughing
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