I could be wrong because I'm new here to, but you should probably get the naphtha down to about 100-150 ml then put it back in the freezer.
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happy camper may be right, just evap 10-20% and re-freeze. or just let evaporate completely if you have a place to do so, they take about the same time, at least for swim's foaf. plus swim's foaf never got a good freeze precipitate, now he just uses the fasa tek instead of freezing or evaporating. good luck, just don't get rid of the naphtha, there is dmt in there. PEACE
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SWIM put it in a Pyrex dish and has gotten it to freeze to white, but when left out it just turns into an oily mess on the bottom of the pan. Half of this has done that and the other half is still the frozen parts. 
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Are you letting the naptha warm up? that will cause the DMT to re dissolve. By allowing this message to pass through your cornea, into your retina, you accept it as is and agree to my disclaimer regarding my posts that they are a complete falsification by doing so freeing me of all liability, direct, indirect, consequential or incidental that may arise from the instillation of this post in your memory bank.
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Just did that and it still all turned into a runny mess. Nothing really to scrape because it just dissolved when left out
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also, you said some things that make it seem like you think the naptha is supposed to evaporate in the freezer. the naptha should be sealed air tight to prevent any condensation getting inside of it. also, make sure you leave it in the freezer for a long enough time, and when you pour the naptha out of the container you can also turn the container upside down to get the naptha to drip off of the crystals. what swim does is uses pint jars for his freeze precip, laying them on their side in the freezer, and when ready, pours all the naptha in another empty jar, takes the jars with the crystals, lay them at an angle to get the naptha to drip off, and place a fan on them to dry them immediately, to prevent much from redisolving.
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