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Scraping of residues from evaporation dish? Options
 
m3dt3ch
#1 Posted : 1/1/2023 10:17:05 PM
Hi all,

I'm close to finishing the evaporations of an acetone extract of LSA seeds and wanted to know whats the best way of scraping up the dried residue? I'm wary of taking a razor to the awkwardly curved evaporation basin, though if it is the only or most approved method I can be careful / gentle doing so. I do have a curved scalpel for woodworking which hasn't been used, that may work well for it.

Thank you
 
downwardsfromzero
ModeratorChemical expert
#2 Posted : 1/2/2023 12:28:11 AM
Sounds about right. Redissolve any remaining, hard-to-scrape crystals and evaporate again in a more favourably shaped container.

Make sure your scalpel is free of grease, is all I can suggest on top of this.




“There is a way of manipulating matter and energy so as to produce what modern scientists call 'a field of force'. The field acts on the observer and puts him in a privileged position vis-à-vis the universe. From this position he has access to the realities which are ordinarily hidden from us by time and space, matter and energy. This is what we call the Great Work."
― Jacques Bergier, quoting Fulcanelli
 
m3dt3ch
#3 Posted : 1/2/2023 5:39:23 PM
downwardsfromzero wrote:
Sounds about right. Redissolve any remaining, hard-to-scrape crystals and evaporate again in a more favourably shaped container.

Make sure your scalpel is free of grease, is all I can suggest on top of this.


Good shout with the grease, I'd have forgotten about it and they are quite greasy. And thanks for the reassurance, it all scraped up really cleanly and was much easier than anticipated. The curve of the blade was perfect for the bowl, pretty much nothing left at all.
 
 
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