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STB
Naptha not separating after mixing Options
 
aetherbound
#1 Posted : 10/25/2022 4:29:47 PM
Hello All,
I'm doing an STB on four 250 gm batches. 250gm MHRB plus 300 gms lye and 1000ml of water. On my second extraction on the first two batches and the naptha is no longer going to the top. Any advice is appreciated, don't remember having this issue before.
In all chaos there is a cosmos, in all disorder a secret order..Jung
All above writing with the exception of Dr. Jung's quote is pure mushroom encrusted cowpie!
 
Voidmatrix
Welcoming committeeModerator
#2 Posted : 10/25/2022 4:39:50 PM
Sounds like emulsion. Heat the soup in a water bath at a lowish temp for a couple hours. Lid off.

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doubledog
#3 Posted : 10/25/2022 4:52:10 PM
If heating doesnt help, add some water to dilute it, 1000ml water per 250 g of bark seems too thick to me.
 
aetherbound
#4 Posted : 10/25/2022 6:01:58 PM
Thanks! I usually heat on third extraction, I'll move it up on one and see what that yields!
Namaste
In all chaos there is a cosmos, in all disorder a secret order..Jung
All above writing with the exception of Dr. Jung's quote is pure mushroom encrusted cowpie!
 
downwardsfromzero
ModeratorChemical expert
#5 Posted : 10/25/2022 6:34:50 PM
doubledog wrote:
If heating doesnt help, add some water to dilute it, 1000ml water per 250 g of bark seems too thick to me.

This. Also, committing 250g bark to an extraction and fouling it up is a good illustration of how it's perhaps better to stick to smaller batches...




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― Jacques Bergier, quoting Fulcanelli
 
aetherbound
#6 Posted : 10/25/2022 6:53:06 PM
Double checked and I used 1500ml, it is soupy enough to pass thru a separatory funnel , it was powdered MHRB. First extract without re-x is at 2.3 grams light yellow, fluffy and soooo floral schmelling. I highly recommend buying a good lab evaporative dish, I was tired of glass casserole dishes with uneven bottoms.Smile
In all chaos there is a cosmos, in all disorder a secret order..Jung
All above writing with the exception of Dr. Jung's quote is pure mushroom encrusted cowpie!
 
 
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