Trickster wrote:And 5-MeO-DMT from Melatonin. Wow!  
|
|
|
Trickster wrote:And 5-MeO-DMT from Melatonin. i'd have some cognitive dissonance observing the flask of 5-meo-dmt under my vacuum, like, "no, its not there"
|
|
|
Espurrr wrote:Trickster wrote:And 5-MeO-DMT from Melatonin. i'd have some cognitive dissonance observing the flask of 5-meo-dmt under my vacuum, like, "no, its not there" There is no vacuum. It is in a small beaker. Do not seek the truth, just drop your opinions.
|
|
|
when spinnin down the dcm using a rotary vane pump, I felt spaced out for a couple mins. could’ve just been the solvent vapors, but wasn’t placebo "Nothing is true, everything is permitted." ~ hassan i sabbah
"Experiments are the only means of attaining knowledge at our disposal. The rest is poetry, imagination." -Max Planck
|
|
|
benzyme wrote:when spinnin down the dcm using a rotary vane pump, I felt spaced out for a couple mins. could’ve just been the solvent vapors,
but wasn’t placebo Rotary vane pump? Were you pumping the rotovap? Too much vacuum, I think. If you did not have a cold trap between the pump and the system some DCM was unable to liquefy in the condenser and was pumped into your lab environment. I saw that happening even with a 2-stage diaphragm pump at vacuum around 300 mbar or less. There is a definite smell of DCM in the air. Usually I remove most of DCM at 500 mbar and 35-37C. The higher the temp and the pressure, the better, because the water feeding the rotovap condenser is around 12C these days and I need the temp difference to be as high as possible for the condenser to work efficiently. When the DCM stops dripping from the rotovap condenser I gradually lower the pressure to ~10-15 mbar (my diaphragm pump would not go lower than that and I am too lazy to switch to a rotary vane). P.S. Sorry for telling some obvious things to real chemists, but it could be of some help to aspiring ones. Do not seek the truth, just drop your opinions.
|
|
|
yeah, I would partially close the vac reg. valve, open the coldfinger condenser valve, evacuate for a few secs, then close the condenser valve. "Nothing is true, everything is permitted." ~ hassan i sabbah
"Experiments are the only means of attaining knowledge at our disposal. The rest is poetry, imagination." -Max Planck
|
|
|
Found this in the debris of a school which gonna be raze soon. A bit of cleaning and it's time to start a new extraction  DansMaTete attached the following image(s):  20190112_163956.jpg (4,277kb) downloaded 405 time(s).« I love the smell of boiling MHRB in the morning »
|
|
|
  "Nothing is true, everything is permitted." ~ hassan i sabbah
"Experiments are the only means of attaining knowledge at our disposal. The rest is poetry, imagination." -Max Planck
|
|
|
the Cerilliant standard above shows a parent ion peak at 189.125 m/z (the mass specs at work are triple-quads, much higher resolution). this is my sample, and my spectra. benzyme attached the following image(s): IMG_5907.jpg (1,763kb) downloaded 362 time(s). IMG_5895.jpg (2,164kb) downloaded 364 time(s)."Nothing is true, everything is permitted." ~ hassan i sabbah
"Experiments are the only means of attaining knowledge at our disposal. The rest is poetry, imagination." -Max Planck
|
|
|
Giant Buddha watching the sunset, Maui. Loveall attached the following image(s): IMG_20190210_171736952.jpg (6,002kb) downloaded 333 time(s).
|
|
|
First picture of a black hole released today by the NSF 🕳 Loveall attached the following image(s): 10BLACKHOLEPHOTO-jumbo-v3.jpg (15kb) downloaded 297 time(s).
|
|
|
Hmmm, black holes and lots of pretty 5-meo on the same page! Coincidence? I think not!!! -the 5 is there, you are not. Sine experientia nihil sufficienter sciri potest -Roger Bacon
*γνῶθι σεαυτόν*
|
|
|
null24 wrote:Hmmm, black holes and lots of pretty 5-meo on the same page!
Coincidence? I think not!!! And buddha too 
|
|
|
Loveall wrote:First picture of a black hole released today by the NSF 🕳 6 billion suns. The weight of our sun in relation to that thing is about equal to yours or mine in relation to that of the whole of mankind. 
|
|
|
The two prints I made today. 60" x 39" each I love commissions like this. JKW attached the following image(s): IMG_7856.jpg (1,535kb) downloaded 260 time(s).
|
|
|
The other print. JKW attached the following image(s): IMG_7857.jpg (1,579kb) downloaded 257 time(s).
|
|
|
t peruv from companion about 3.5ft now ○ attached the following image(s): trr.jpg (131kb) downloaded 178 time(s).
|
|
|
Sunspot details captured by the big bear solar observatory. Loveall attached the following image(s): 59614543_2145364612166814_8485960052308443136_n.jpg (118kb) downloaded 180 time(s).
|
|
|
it ain't honey oil  "Nothing is true, everything is permitted." ~ hassan i sabbah
"Experiments are the only means of attaining knowledge at our disposal. The rest is poetry, imagination." -Max Planck
|
|
|
Big bloom from a (species?) Trich and a single bloom from an Echinopsis "Don Juan" Wolfnippletip attached the following image(s): cactuspcflowers2,5.30.19.jpg (136kb) downloaded 439 time(s). thumbnail (1).jpg (73kb) downloaded 440 time(s).My flesh moves, like liquid. My mind is cut loose.
|