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Extraction of shrooms Options
 
amor_fati
Chemical expertSenior Member
#61 Posted : 4/5/2009 5:11:21 AM
So could one say that psilocybin is bioactive, while psilocin is pychoactive?

Also, 69ron, SWIM tried that steaming method along with a decent dose of ascorbic, and it seemed to make his mushrooms nearly twice as active. He still got headaches toward the end, but they were greatly lessened.
 
69ron
#62 Posted : 4/5/2009 5:16:05 AM
It's a cool trick. I wish I knew exactly what it works. It's definitely effective.

Other than the increase in potency and lessoning of your headache, did you notice any other differences in effects after the steam treatment?
You may remember me as 69Ron. I was suspended years ago for selling bunk products under false pretenses. I try to sneak back from time to time under different names, but unfortunately, the moderators of the DMT-Nexus are infinitely smarter than I am.

If you see me at the waterpark, please say hello. I'll be the delusional 50 something in the American flag Speedo, oiling up his monster guns while responding to imaginary requests for selfies from invisible teenage girls.
 
amor_fati
Chemical expertSenior Member
#63 Posted : 4/5/2009 6:26:51 AM
69ron wrote:
It's a cool trick. I wish I knew exactly what it works. It's definitely effective.

Other than the increase in potency and lessoning of your headache, did you notice any other differences in effects after the steam treatment?


Well, I suppose for SWIM, the level of hallucinations and quality of the body high are synonymous with the level of potency in terms of psilocybes. SWIM would say that the hallucinations were more engulfing, and he felt much more creatively inspired and motivated than he has on any other psilotrip.

SWIM would think that though psilocybin is probably nice to have in smaller quantities, it can be too much in larger. With psilocin (or perhaps other analogs) on the other hand, the skies the limit.
 
psychosisdoses
#64 Posted : 4/5/2009 6:42:31 AM
hmm this steam treatment sounds interesting

elaborate please

im guessing it converts some of the psylocybin into psilocin
seems like itd be the thing to do
"once youve locked yourself into a serious drug collection the tendency is to push it as far as you can..." - hunter s. thompson

~~~~~~~~...You are me and i am you, i will always be with you...~~~~~~~~IAmUsWeYouMe~~~~~~~~
‹maxzar100› YOU are like acid
‹mattimus› dosesdosingdoses
 
69ron
#65 Posted : 4/5/2009 8:57:22 AM
You steam cook the dried mushrooms until they lose all their blue color. The theory is that this destroys all the enzymes that turn psilocin blue, so it protects the psilocin content in the mushrooms, while at the same time hydrolyzing all the psilocybin into psilocin. Whatever it actually does, it definitely improves the potency quite a bit.
You may remember me as 69Ron. I was suspended years ago for selling bunk products under false pretenses. I try to sneak back from time to time under different names, but unfortunately, the moderators of the DMT-Nexus are infinitely smarter than I am.

If you see me at the waterpark, please say hello. I'll be the delusional 50 something in the American flag Speedo, oiling up his monster guns while responding to imaginary requests for selfies from invisible teenage girls.
 
Phlux-
Chemical expertSenior Member
#66 Posted : 4/5/2009 9:31:08 AM
okay so there was a slight stuffup - swim overshot the mark on the ph - all was going fine till the very end - swim worked very fast from that point on to try extract the active before it degraded too much - anyway swims combined 3 naptha pulls are evapping slightly before fp and it is producing a huge amount of white when blown on so it looks promising. 3 xylene pulls were also done after that, emulsions were a bit of a problem - but we will see.
antrocles wrote:
...purity of intent....purity of execution....purity of experience...

...unlike the "blind leading the blind". we are more akin to a group of blind-from-birth people who have all simultaneously been given the gift of sight but have no words or mental processing capabilites to work with this new "gift".

IT IS ONLY TO THE EXTENT THAT WE ARE WILLING TO EXPOSE OURSELVES OVER AND OVER AGAIN TO ANNIHILATION THAT WE DISCOVER THAT PART OF OURSELVES THAT IS INDESTRUCTIBLE.


Quote:
‹Jorkest› the wall is impenetrable as far as i can tell


Quote:
‹xtechre› cheese is great


He who packs ur capsules - controls your destiny.

 
Phlux-
Chemical expertSenior Member
#67 Posted : 4/5/2009 2:33:38 PM
this is not precipping out of the solution, if swim takes it out the freezer its clear - blow on it pieces almost drop out and surface layer of white appears - how should swim get it out of the naptha ? - evap further(heat/lignt?) then try again ?
antrocles wrote:
...purity of intent....purity of execution....purity of experience...

...unlike the "blind leading the blind". we are more akin to a group of blind-from-birth people who have all simultaneously been given the gift of sight but have no words or mental processing capabilites to work with this new "gift".

IT IS ONLY TO THE EXTENT THAT WE ARE WILLING TO EXPOSE OURSELVES OVER AND OVER AGAIN TO ANNIHILATION THAT WE DISCOVER THAT PART OF OURSELVES THAT IS INDESTRUCTIBLE.


Quote:
‹Jorkest› the wall is impenetrable as far as i can tell


Quote:
‹xtechre› cheese is great


He who packs ur capsules - controls your destiny.

 
benzyme
Moderator | Skills: Analytical equipment, Chemical master expertExtreme Chemical expert | Skills: Analytical equipment, Chemical master expertChemical expert | Skills: Analytical equipment, Chemical master expertSenior Member | Skills: Analytical equipment, Chemical master expert
#68 Posted : 4/5/2009 3:37:47 PM
don't heat once the psilocin is in the naptha.
pour off some of the naptha to slow evap, and put the rest back in the freezer.

eventually, there will be a dark green residue when scraped. this is crude psilocin...one can recrystallize with heptane (like with dmt), but it's noticeably tougher to get it to crystallize. no worries. the residue is still very active...cap it, or take with your fav juice.
"Nothing is true, everything is permitted." ~ hassan i sabbah
"Experiments are the only means of attaining knowledge at our disposal. The rest is poetry, imagination." -Max Planck
 
Phlux-
Chemical expertSenior Member
#69 Posted : 4/5/2009 5:01:48 PM
evap it it further then fp it ? or evap it all ? - sorry not to clear on ur last post.
antrocles wrote:
...purity of intent....purity of execution....purity of experience...

...unlike the "blind leading the blind". we are more akin to a group of blind-from-birth people who have all simultaneously been given the gift of sight but have no words or mental processing capabilites to work with this new "gift".

IT IS ONLY TO THE EXTENT THAT WE ARE WILLING TO EXPOSE OURSELVES OVER AND OVER AGAIN TO ANNIHILATION THAT WE DISCOVER THAT PART OF OURSELVES THAT IS INDESTRUCTIBLE.


Quote:
‹Jorkest› the wall is impenetrable as far as i can tell


Quote:
‹xtechre› cheese is great


He who packs ur capsules - controls your destiny.

 
Maxax
#70 Posted : 4/5/2009 5:05:25 PM
Nice to know some people are as interested in psychedelics as I am . If your tek works could you write a clear tek ? Thanks in advance
 
benzyme
Moderator | Skills: Analytical equipment, Chemical master expertExtreme Chemical expert | Skills: Analytical equipment, Chemical master expertChemical expert | Skills: Analytical equipment, Chemical master expertSenior Member | Skills: Analytical equipment, Chemical master expert
#71 Posted : 4/5/2009 5:11:20 PM
Phlux- wrote:
evap it it further then fp it ? or evap it all ? - sorry not to clear on ur last post.


pour some of your psilocin-containing naptha into a dish, and let evap;
the rest you can put back in the freezer. when the solvent in the dish has evaporated, repeat.
"Nothing is true, everything is permitted." ~ hassan i sabbah
"Experiments are the only means of attaining knowledge at our disposal. The rest is poetry, imagination." -Max Planck
 
Phlux-
Chemical expertSenior Member
#72 Posted : 4/5/2009 5:15:03 PM
thanks
antrocles wrote:
...purity of intent....purity of execution....purity of experience...

...unlike the "blind leading the blind". we are more akin to a group of blind-from-birth people who have all simultaneously been given the gift of sight but have no words or mental processing capabilites to work with this new "gift".

IT IS ONLY TO THE EXTENT THAT WE ARE WILLING TO EXPOSE OURSELVES OVER AND OVER AGAIN TO ANNIHILATION THAT WE DISCOVER THAT PART OF OURSELVES THAT IS INDESTRUCTIBLE.


Quote:
‹Jorkest› the wall is impenetrable as far as i can tell


Quote:
‹xtechre› cheese is great


He who packs ur capsules - controls your destiny.

 
Phlux-
Chemical expertSenior Member
#73 Posted : 4/5/2009 8:40:51 PM
okay evap of naptha done and not much of a yeild -
3 xylene pulls were done after the naptha pulls - how should swim salt out the psilocin - if there is any in there.
antrocles wrote:
...purity of intent....purity of execution....purity of experience...

...unlike the "blind leading the blind". we are more akin to a group of blind-from-birth people who have all simultaneously been given the gift of sight but have no words or mental processing capabilites to work with this new "gift".

IT IS ONLY TO THE EXTENT THAT WE ARE WILLING TO EXPOSE OURSELVES OVER AND OVER AGAIN TO ANNIHILATION THAT WE DISCOVER THAT PART OF OURSELVES THAT IS INDESTRUCTIBLE.


Quote:
‹Jorkest› the wall is impenetrable as far as i can tell


Quote:
‹xtechre› cheese is great


He who packs ur capsules - controls your destiny.

 
benzyme
Moderator | Skills: Analytical equipment, Chemical master expertExtreme Chemical expert | Skills: Analytical equipment, Chemical master expertChemical expert | Skills: Analytical equipment, Chemical master expertSenior Member | Skills: Analytical equipment, Chemical master expert
#74 Posted : 4/6/2009 1:25:41 AM
if SWIY wants to salt it out, SWIY would need to acidify it.

this is where OJ would come in handy. psilocin free base is very soluble in acidic water, and would be converted into citrate salts, and oj also has ascorbic acid to preserve the psilocin.

just remember to make sure the naptha is completely evaporated. the product will be resinous, but it's safe.
"Nothing is true, everything is permitted." ~ hassan i sabbah
"Experiments are the only means of attaining knowledge at our disposal. The rest is poetry, imagination." -Max Planck
 
Phlux-
Chemical expertSenior Member
#75 Posted : 4/6/2009 8:31:15 AM
okay well the evap left behind very very little residue - if salting out of the xylene - swim would like to use hcl, fumaric acid or something along those lines - what would be best ?
antrocles wrote:
...purity of intent....purity of execution....purity of experience...

...unlike the "blind leading the blind". we are more akin to a group of blind-from-birth people who have all simultaneously been given the gift of sight but have no words or mental processing capabilites to work with this new "gift".

IT IS ONLY TO THE EXTENT THAT WE ARE WILLING TO EXPOSE OURSELVES OVER AND OVER AGAIN TO ANNIHILATION THAT WE DISCOVER THAT PART OF OURSELVES THAT IS INDESTRUCTIBLE.


Quote:
‹Jorkest› the wall is impenetrable as far as i can tell


Quote:
‹xtechre› cheese is great


He who packs ur capsules - controls your destiny.

 
benzyme
Moderator | Skills: Analytical equipment, Chemical master expertExtreme Chemical expert | Skills: Analytical equipment, Chemical master expertChemical expert | Skills: Analytical equipment, Chemical master expertSenior Member | Skills: Analytical equipment, Chemical master expert
#76 Posted : 4/6/2009 1:32:55 PM
ascorbic.

the whole deal with psilocin is its tendency to degrade. the OH group (which dmt lacks) needs to be protected by an antioxidant. none of the traditional acids used (acetic, hydrochloric, fumaric, sulfuric) will protect the hydroxy group.

you could still convert to a salt with those acids, just store it like you would store the free base...away from light and air exposure (long term)
"Nothing is true, everything is permitted." ~ hassan i sabbah
"Experiments are the only means of attaining knowledge at our disposal. The rest is poetry, imagination." -Max Planck
 
Phlux-
Chemical expertSenior Member
#77 Posted : 4/6/2009 1:45:02 PM
thanks.
if swim adds ascorbic acid - disolved in water - will the psilocin precip out of the solution or does it need to be separated then evaporated as with mesc hcl saltings, then washed ?
antrocles wrote:
...purity of intent....purity of execution....purity of experience...

...unlike the "blind leading the blind". we are more akin to a group of blind-from-birth people who have all simultaneously been given the gift of sight but have no words or mental processing capabilites to work with this new "gift".

IT IS ONLY TO THE EXTENT THAT WE ARE WILLING TO EXPOSE OURSELVES OVER AND OVER AGAIN TO ANNIHILATION THAT WE DISCOVER THAT PART OF OURSELVES THAT IS INDESTRUCTIBLE.


Quote:
‹Jorkest› the wall is impenetrable as far as i can tell


Quote:
‹xtechre› cheese is great


He who packs ur capsules - controls your destiny.

 
Maxax
#78 Posted : 4/6/2009 4:27:42 PM
Could you post pics of the final yield ? And about how potent the stuff is

Thx
 
benzyme
Moderator | Skills: Analytical equipment, Chemical master expertExtreme Chemical expert | Skills: Analytical equipment, Chemical master expertChemical expert | Skills: Analytical equipment, Chemical master expertSenior Member | Skills: Analytical equipment, Chemical master expert
#79 Posted : 4/6/2009 5:21:55 PM
Phlux- wrote:
thanks.
if swim adds ascorbic acid - disolved in water - will the psilocin precip out of the solution or does it need to be separated then evaporated as with mesc hcl saltings, then washed ?


just a slow evap.
the product may be resinous, but it will be stable enough for long-term storage.

it probably won't precip in the water-ascorbic acid solution. the free base will bind to the ascorbate ions in solution, and the psilocin will be in the form of water-soluble psilosin ascorbate. after the water evaporates, what will be left is the fairly stable salt
"Nothing is true, everything is permitted." ~ hassan i sabbah
"Experiments are the only means of attaining knowledge at our disposal. The rest is poetry, imagination." -Max Planck
 
Maxax
#80 Posted : 4/8/2009 3:25:08 AM
Any news Phlux or tripping your balls off ? Razz
 
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