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SWIM has crystals!!......now what? *Pics added* Options
 
corridors of my cells
#21 Posted : 9/28/2009 11:44:32 PM
is this the total stuff in the vial all you got out of 100gr? is that a 1 dram(3.5g) vial? hmm if it is you had far less than i got from 50gr. and you used 2 times naoh when you consider the amount of mhrb we used :S hmmm weird. it looks so clean tho. Nice yield, enjoy your trips my friend Smile
 
Methtical
#22 Posted : 9/28/2009 11:51:00 PM
That is a 5ml vial, and pretty much yes it is the total, discounting the glass-shard crystals SWIM has forming slowly in the evaporating re-x.

SWIM realises it is not the best yield in the world, however, as SWIM said before, there were lessons learned during the first run that he is sure will help produce a more bountiful yield in subsequent extractions in the future. SWIM is glad he got this on the first attempt given that he has seen threads where people have attemped multiple times and not even come close, or had spice that wasn't as aesthetically pleasing.

SWIM thanks everyone and shall greet you in the cosmos!

Methtical
 
Bill Cipher
#23 Posted : 9/29/2009 3:29:35 AM
Good work. A .06-.07% yield is not a bad result.

The brown crud may be some of the basified solution. More likely, if you didn't notice it before, it's DMT-oxide, or it may very well just be plant fats/oils. Chances are, it's a bit of all of the above. Separate as much of it as you can, but a bit of color won't kill you. Try heptane for your next re-x. It's a much better option.
 
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