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My Extraction Method. Options
 
Spiced
#1 Posted : 9/20/2009 11:01:44 AM
I found an easy and good way to extract a high yield of pure white crystals, it takes some patience, but the reward is huge.

-Find a jar that fits about 3 litres.
-Hexane, or Naptha.
-Lye or something like it (granulated).
-Mimosa Hostilis (pre powdered is fine).
-3 or 4 collection jars.
-Pipette, or an improvised one.

-Now put 2.25 litres of water in the jar and ad 100 g. of granulated Lye/NaOH to it, then ad 100 g. of pre powdered Mimosa Hostilis, mix it untill everything is dissolved, close it, and put the jar away for 24 hours, less is good too, but 24 hours will give better results.

-Now, after 24 hours open the jar and ad 100 ml. Naptha/Hexane/Heptane, close the jar and roll it gently -(do not shake, you don't want emulsions)- around for 10 minutes (you can do less, but again, for better results 10 minutes is advised).

-let possible emulsions fade away, and roll the jar again for another 10 minutes.

-Repeat this one more time, so you rolled that jar for 30 minutes, let possible emulsions fade away, and open the jar to extract the top layer of Naptha, put this Naptha in one of your collection jars and put that jar in the freezer.

-Now repeat all of this again, ad 100 ml. Naptha, and roll that jar again, this time 8 minutes is fine, do this as you did before, so you have rolled the jar for 24 minutes, again extract the top layer, and put it in another collection jar in the freezer.

-Ad 100ml. of Naptha and repeat the whole process again, this time 6 minutes is fine, so after approximatly 18 minutes of jar rolling you can extract the last layer and collect it in another third jar, you can put that in the freezer aswell.


-Best is to leave the jars in the freezer for 48 hours, after 24 hours you could collect your yield, but if you wan't a higher yield be patient and wait 24 hours more, do not disturb or shake the jars when they are in the freezer!

-After 48 hours you can take them out, and take another jar, put a coffee filter in it, and empty the collection jars in that filter, put the remaining Naptha in a jar, you can re-use it for later extractions.

-Let the crystals dry out, cut possible chunks with a razorblade into small pieces, and let them dry out completely, so all Naptha is evaporized.


There will still be some residue in the collection jars, but this will get oily when you'll try to scrape it out, best is to re-crystalize the residue.

The collected crystals don't need to be re-crystalized if you have only extracted the Naptha, without any brown sludge, otherwise you can re-crystalize.

-Using this method should get you an amount of 0.6 g. white crystals of DMT.

I tried 4 different methods, and this worked out the best by far.
Also, it's best to store the collection jars in the fridge for an hour before putting them in the freezer, by doing this the jars will cool down more slowly, wich will produce more crystals aswell, also make sure your freezer is on it's maximum capacity, the colder the better.


Peace. Smile
 
L_Star
#2 Posted : 9/21/2009 7:16:38 PM
hello Spiced swim wanted to ask is that 100g or 100mg of mimosa?

respect n regards L Star


Much respect to all from L_Star

Disclaimer: EVERYTHING posted by L_Star is said from the following persons: SWIM. All are hypothetical posts and are not endorsements of any activities, beliefs, and practices stated, that may be correlated with the person stated, or another person posting, or third party user, in anyway on dmt-nexus.com. All that is said is for educational purposes and as said is "hypothetical" and therefore cannot be taken for true accounts. SWIM and L_Star abide by the Law in all practices. SWIM would like reader to note that SWIM is blind, and L_Star is a typing assistant voluntering for SWIM. L_Star is bound by legal legislation for customer privacy by Data Protection Act, therefore SWIM will not be identified.

Regards L_Star
 
dread
#3 Posted : 9/21/2009 7:36:14 PM
Obviously it's 100g. The mg is a typo.

Anyway this doesn't differ much from the standard STB teks, IMO...

And I've always had better results with A/B. So thank you but I'll pass...
 
Opiyum
#4 Posted : 9/21/2009 9:24:04 PM
SO the only real difference from noman's is the ratio of lye to bark and the length of time you disturb the mixture. A bit longer in the freezer too I guess.
What do you attribute to the good yield? Could have just been good bark or have you used other methods with the same bark to compare?
 
Jorkest
Moderator | Skills: Extraction Troubleshooting, (S)elf ProgrammingChemical expert | Skills: Extraction Troubleshooting, (S)elf Programming
#5 Posted : 9/22/2009 1:03:39 PM
if 0.6% is good yield...i would say go back and extract some more from you bark...SWIM has never had a good yield that low
it's a sound
 
Phlux-
Chemical expertSenior Member
#6 Posted : 9/22/2009 1:43:53 PM
yeah 800mg from 50g bark is about average - should be getting at least a bare minimum of 1% - looks like its time to either do jorkests tek or a fasa tek.
antrocles wrote:
...purity of intent....purity of execution....purity of experience...

...unlike the "blind leading the blind". we are more akin to a group of blind-from-birth people who have all simultaneously been given the gift of sight but have no words or mental processing capabilites to work with this new "gift".

IT IS ONLY TO THE EXTENT THAT WE ARE WILLING TO EXPOSE OURSELVES OVER AND OVER AGAIN TO ANNIHILATION THAT WE DISCOVER THAT PART OF OURSELVES THAT IS INDESTRUCTIBLE.


Quote:
‹Jorkest› the wall is impenetrable as far as i can tell


Quote:
‹xtechre› cheese is great


He who packs ur capsules - controls your destiny.

 
PerPLexED
#7 Posted : 9/22/2009 3:17:15 PM
Pretty much a simplified STB.
High Yield extraction method: 4 pulls naptha, 4 pulls xylene.
"We are the analogies we believe." - PerPLexED

PerPLexED is a confused fictional creature.
He doesn't know that he is fictional.
He doesn't know what fiction is.
He doesn't know anything, really.
But strives to know it all.
 
Spiced
#8 Posted : 9/26/2009 8:36:25 PM
Oh shit, and i was already happy with this amount, so i could do a lot better then?
Hmmm, i'm a bit de-motivated now, lol. Confused

I have still some residue in the jars that i didn't count with them, maybe i should extract some more next time, thanks though.



BTW it should be noticed that this is not actually MY tek, it's just the method i like to use, it's based on other teks with a little modification, sorry if it is somehow misleading.
 
soulfood
Senior Member | Skills: DMT, Harmaloids, Bufotenine, Mescaline, Trip advice
#9 Posted : 9/27/2009 12:17:22 AM
I'd say 24 hours for a soak with the NaOH is the minimal amount to wait. Try give it 3 days.

1.5% is as low as I expect for a yield, that's not including N-oxides.
 
Spiced
#10 Posted : 9/27/2009 9:57:09 AM
Damn, so you get 1.5 gr. out of 100 gr. mimosa? Shocked
What tek do you use if i may ask?


Brrr. i'm changing the topic title to my extraction method, 0.6 seems to be anything but a high yield. Confused
 
Spiced
#11 Posted : 10/3/2009 5:18:40 PM
Jorkest wrote:
if 0.6% is good yield...i would say go back and extract some more from you bark...SWIM has never had a good yield that low



As adviced i did another 3 pulls and got approximatly 500 mg. extra out of it, 200 mg. white crystals where left in the coffee filter, and today i found another 300 mg. yellowish crystals that where left in the collection jars, i forgot about the jars for a week, today i scraped them out and was supprised that there was still such a nice amount of DMT left in there. Razz

But ok, it's still a pretty low yield i assume, but i'm happy with it for now.
 
 
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