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JohnIce2
#1 Posted : 2/29/2016 12:17:19 AM
Made this using the straight to base method with Chaliponga. Pulled with 70% rubbing alcohol (IPA) which was then "salted out" to defat and purify the solution as well as separating the water from the alcohol (IPA then became 99%).
Defated product was then evaped and tested (it worked fine, no breakthrough, nice OEVs and a feeling of being so high that your in space). That product which was oarngeish brown in color and waxy as well was then redissolved in IPA and water was added, then salt, and the solution was given time to separate. That layer of IPA was strained through a filter (Coffee filter) and then put in a shot glass over a open flame on low until it crystallized. Crystals appeared white at first but then turned a light greenish color. My IPA solutions were a green color after they were pulled and filtered (although it was in reality so yellow that it appeared green and then if it was left long enough the yellow intensified to a point where it looked red).

So what you think? That was a Sum up of my process. I think that the green is residual chlorophyll yet to be removed from solution.

JohnIce2 attached the following image(s):
IMG_1557.JPG (899kb) downloaded 85 time(s).
All posts are imaginary and are just examples for me to learn simple to advanced organic chemistry processes.
 
slewb
#2 Posted : 2/29/2016 2:03:02 AM
When you say "salted out" do you just mean that you added salt to the IPA? Add water to your crystals and see if they dissolve.
 
JohnIce2
#3 Posted : 2/29/2016 2:13:03 AM
Yes haha, the site I found the info about the IPA on called the method "Salting Out".

and ok!. Will this disolve my alkaloids tho? cause it is a bitch for me to evap stuff. exspecially water. Honestly I believe its just Chlorphyl tainted Spice. Has a kind of Lime Yellow tint to it but still a noticable white to a degree (the pic doesnt capture these aspects as well). I know its active cause ive been using it in liquid vape form (still in the IPA solution, not crystals straight into PG/VG vape juice).
All posts are imaginary and are just examples for me to learn simple to advanced organic chemistry processes.
 
JohnIce2
#4 Posted : 2/29/2016 2:57:26 AM
Ok so I tested a very small amount of the crystals. They appear to spread out within the water, but not dissolve. Just separate from each other and spread. Made the water look cloudy white.
All posts are imaginary and are just examples for me to learn simple to advanced organic chemistry processes.
 
dreamer042
Moderator | Skills: Mostly harmless
#5 Posted : 2/29/2016 5:10:37 AM
JohnIce2 wrote:
That layer of IPA was strained through a filter (Coffee filter) and then put in a shot glass over a open flame on low until it crystallized.

Stop

Stop right there.

Flammable solvent over open flame? Confused

Time to review lab safety 101.
Row, row, row your boat, Gently down the stream. Merrily, merrily, merrily, merrily...

Visual diagram for the administration of dimethyltryptamine

Visual diagram for the administration of ayahuasca
 
JohnIce2
#6 Posted : 2/29/2016 5:49:31 AM
Embarrased Yeah u got me their haha. Guess i'm lucky nothin happened ( I use a vent hood device that sucks up the fumes before they can fall toward the flame and ignite. Same thing my high school Chemistry teacher used to due when heating flamable stuff. ). Ill review the safety procedures, but I did find a safer way to do it. I got a hot plate and made sure it was below the flash point of 99% IPA on the temperature scale.

Anyways, can anyone tell me what they think I have here? I've smoked some (Dissolved in vape fluid) and mixed it with some Green I had and I am indeed tripping. Shadows are all weird and everything is shimmering in a rainbow light texture. Strong Mental effects were noticed, and physical effects ranged from numbness to tingly sensations. Here and their I'll start to hear high pitch frequencies that feel like they are coming from the center of my head. Sorry if any of this sounds crazy.... lol
All posts are imaginary and are just examples for me to learn simple to advanced organic chemistry processes.
 
 
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