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Is this the correct place to ask about recrystallization techniques? Options
 
Ronin175k
#1 Posted : 5/18/2015 8:42:35 PM
Apologies in advance. Anyone that can help me understand a couple things or if you can point me to the correct area... Thanks
 
a1pha
Moderator | Skills: Master hacker!
#2 Posted : 5/18/2015 8:49:12 PM
It would be easier to answer if we knew the question.

Also, check out the "chat" link above. Members there can sometime assist with basic questions.
"Facts do not cease to exist because they are ignored." -A.Huxley
 
Ronin175k
#3 Posted : 5/18/2015 10:00:10 PM
thanks for the response...

After the extraction naptha/ heptane wash... to recrystallize, is the process to backsalt then redissolve in solvent (which solvent) and then to slow cool to bring it back, filter/finish?

or what are the correct steps and or solvents to use?

I am going with:

300ml Deionized water
6g Sodium hydroxide
30g MHRB

Naptha
Heptane

(for the initial extraction)

or should a noob just start with a simple A/B. I feel a slight obsession with getting this correct.
I am doing this in dreams and they are telling me I am close. or am I delusional
 
a1pha
Moderator | Skills: Master hacker!
#4 Posted : 5/18/2015 10:59:34 PM
1) You might consider washing before recrystallizing. This helps eliminate any remaining basic solution.
2) With the materials described, Cybs' Hybrid ATB 'Salt' Tek would be a good A/B.
3) To Recrystallize, take a look here.

Feel free to post any specific questions.

Smile
"Facts do not cease to exist because they are ignored." -A.Huxley
 
Ronin175k
#5 Posted : 5/18/2015 10:59:37 PM
Thanks for the help guys....let you know how it turns out

(PS. chatroom helps, noobies!)


Thank you a1pha!
 
Ronin175k
#6 Posted : 5/18/2015 11:12:10 PM
Flow chart is great, A1pha thanks a bunch!
 
a1pha
Moderator | Skills: Master hacker!
#7 Posted : 5/18/2015 11:26:55 PM
Ronin175k wrote:
Flow chart is great, A1pha thanks a bunch!

Thank cyb when you see him. He did a great job with that tek!

Welcome to the DMT-Nexus!
"Facts do not cease to exist because they are ignored." -A.Huxley
 
 
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