Yeah I tried a couple A/B methods. Strong acid -> weak base -> strong base.

I then tries weak acid to strong base.

None of these actually improved the quality of my spice, just slightly lowered my yield. What worked was the simple things, like washing my solvent and using activated carbon.

Never used activated carbon, never even rxd, I just do the mini a/b at the end, I'll have to wait till you post what you do and see what's different

I do a single re-x. I plan on going into great detail on that particular step as well. If done right, product loss is absolutely nominal. And your glass shard will start growing in 5-10 seconds hehehe

Ha can't wait for the write up

sbc 1 ,, if you let the solvent cool down at room temp with no added breeze for roughly three hours then sit a very slight breeze or fan on the precipe dish and let the naps evap fully instead of the freeze precipe you'll get nice big fat heavy shards instead of the fluff Snow White you get with the freeze

Thanks for the info EW I'll try that with the new batch, thanks to both you and cyb for your easy to follow teks, just waiting for the info of you about the volume's for 500g now ha

Have you a ph meter ?? Is so you really don't need measurements or TEKs really !

Just make sure you're liquid isn't thick so it mix's quite well , but remember you will lose a small percentage off you're yeild as the more you extract the more you loose !
Example if I do a 100g TEK I get 1.6% 1.6g so x by 5 = 8g
in theory but if you do a 500g TEK and you get 6.5g that would = 1.3% ya loosing 1.5 g DMT this is IME anyways !!
Now I put this down to focus ! Again example if I'm doing 100g TEK I'm focusing on a smaller bottle thinner neck easier to handle less waste ,, 500g TEK big heavy chunky bottle to throw around that makes for less enthusiasm and more can't wait to bloody finish this thing ! Lol again IME !!

No got litmus paper, yeah was just going to do it in a big bottle, just wanted to no the size I should use, how much water, salt, lye and vinegar I should use