I really didn't know how to word the subject any better to get people to check it out. I'd really like to understand what happened here. I've read all the goo ?s already and I have a good understanding of extraction. Just blasted off into hyperspace yesterday and it was amazing!
I use A/B extraction of acrb and let it evap to goo on pyrex. I keep it in the freezer till ready to scrape in a machine.
IMPORTANT PART: I was ready for a new extraction so I scraped all the goo off the pyrex into a different smaller dish to clean out the large pyrex that I would use for the fresh naphtha pulls. Now when I smoke the stuff I scraped (a dark yellow hardened goo), a get what I would call a jungle/ 5 meo experience. Dark shapes, shifting, and heavy body. I have no real breakthrough and I don't understand why. Has this happened to anyone or does anyone have any theories?
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Apparently going below PH 4 sucks out other alkaloids. Perhaps some heat and open air may have caused dmt to turn to dmt-oxide. Perhaps the solvent you used has other components that sucked out other things with it (xylene).
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Dr. Dimitri wrote:Apparently going below PH 4 sucks out other alkaloids. IMO I don't think this is true at all !!
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Interesting. In the most potent batch: 3 cups vinegar to 1500 ml water. ph was 3. This was a cold 24 hour vinegar soak. Then two pulls of xylene to defat. Then 5 tbsp lye stirred occasionally for 1 hour. Then 3 pulls of naptha. Straight to evaporation.
The only difference in the junk batch was starting with more water, same vinegar, and simmering in crock pot for 24 hours. The ph of that was 4.
Will keep that in mind, though. Still haven't figured out this beast and that is part of the fun.
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Did your ACRB goo after some drying take on this dark yellow wood puty look as pictured below? This shit is very potent and visual!... But there must be some NMT in it with the DMT because Pure is extreemly visual... I never tryed the dry ice method to remove the NMT yet. But. may try in future.. starway6 attached the following image(s):  DSC08034.JPG (2,658kb) downloaded 45 time(s). DSC08036.JPG (3,088kb) downloaded 46 time(s).
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starway6 wrote:Did your ACRB goo after some drying take on this dark yellow wood puty look as pictured below?
This shit is very potent and visual!...
But there must be some NMT in it with the DMT because Pure is extreemly visual...
I never tryed the dry ice method to remove the NMT yet.
But. may try in future.. What a mess ! Starway6 you really should try the MiniAB on the end of you're TEK instead of the defat , you'll be pleasantly surprised ! 
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