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ScriabinAnime
#1 Posted : 2/7/2014 10:38:38 PM
After REMOVED: No talk of Aquiring MHRB, and grinding it into a powder, is it desirable to cold rinse it, relatably to rinsing rice of starch before boiling it, to remove impurities before proceeding to mix with hot water/hot acid/water? Furthermore, in a straight to base extraction, is it more desirable to switch immediately from cold rinsed MHRB powder to very hot/boiling water in order for more dmt to radiate out before mixing with lye base water? [To clarify, does the temperature difference between COLD root bark immediately set to hot or BOILING water/vinigar etc, make a difference BECAUSE it was cold in the first place, thus a greater temperature difference?]

Is adding lye salt 1 grain at a time most desirable?

Is the non polar solvent, such as vm & p naptha and n-heptane, better depending on how non-polar it is? Which non-polar solvent is better then? I've heard heptane extracts more alkaloids and is more non-polar.

Has anyone done experiments to see if acid is worth using or not under proper elemental conditions?


Are any steps, such as evaporation, more useful in pure darkness than ambient light?

Correct me if I'm wrong, but it appears Gibran2 posted some good information.

"
1 ----- Very little if any acid has to be added to the bark powder. I’ve never tried using no acid at all, but as little as 50mL of 5% acetic acid in 2L of water yields the same results as much more. My guess is that most/all of the DMT in MHRB is already in salt form. I bet that acid has little to no effect on yield.

2 ----- Boiling of the acidified solution is totally unnecessary. Some TEKs call for soaking/boiling for hours. I add hot (not boiling) water to the MHRB powder, stir it a few times, then let it settle. I then siphon off the liquid and repeat 3 more times.

3 ----- Filtration is unnecessary. Many TEKs use messy and wasteful filtration procedures to separate the liquid from the MHRB. This is not necessary. Allowing the solution to settle for 30-45 minutes and then siphoning off the clear liquid is a much cleaner and less wasteful way to do separations.

4 ----- Gentle boiling or slow simmering for reduction is not necessary. I do my reductions at a full boil. There is no loss of product that results from vigorous boiling, and over 1L of liquid can be reduced to 200mL in about 15 minutes. Depending on your stove, you might even reduce it faster than that.

5 ----- No separatory funnel is needed. Once the DMT-containing liquid is reduced, it can be processed in the same manner as a STB – the solution in a jar/bottle is basified (using far less base than STB), non-polar solvent is added, and the extraction proceeds like STB. No need for expensive equipment.

These adjustments make for a very quick and easy A/B with very good yields. (I’ve had yields of 1.75% with MHRB from a vendor known for high quality MHRB.)"

If anyone knows all of the elementally most proper ways of extracting dmt, let me know
 
TheAllSeeingEye
#2 Posted : 2/8/2014 4:40:00 AM
Quote:
Is it a good thing to wash mhrb powder with cold water before starting?


Let my cat clarify, that there is tons of information that should answer this question. My cat says to do at least a little research.

Quote:
Is ethanol better than hexane/naptha?


My cat say this depends, if you are insinuating that ethanol is better to drink hexane/naptha than Ethanol is much safer to digest. However can be lethal in high doses and should not operate a motor vehicle.

Quote:
What makes hexane/naptha etc. the "best" for extracting? How do you make the "best" solvent?


My cat told me that that Naptha/hexane has a very weak Dielectric constant.
 
expandaneum
#3 Posted : 2/8/2014 10:11:58 AM
please do some basic research, your asking to be spoon fed.

start your career of self learning here
https://www.dmt-nexus.me....aspx?g=posts&t=1085

take care
Disclaimer:
All Expandeum's notes, messages, postings, ideas, suggestions, concepts or other material submitted via this forum and or website are completely fictional and are not in any way based on real live experience.
 
 
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