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Freeze precip issues, looking for advice Options
 
drigonometry
#1 Posted : 1/26/2014 12:52:50 AM
Hey guys! Followed this tek mostly to a tee

http://elfspice.tripod.c...a/acacia_extraction.html

I ended up with a couple decent first pulls(I did freeze precip to avoid fumes)
But on my 4th or 5th pull i got some water in the baster i was using to pull out solvent with, and after I froze it in a baking dish there were just water crystals that melted in the bottom of the pan after awhile, no DMT that was visible.

So I tried again with the same solvent, sans water, since it all froze on the bottom of the last pull. No luck, no crystals. Tried new solvent, same problem. Just no yield hardly at all if any.

I've only gotten maybe 400-500 mg out of a 250g acacia confusa extraction, should be around 1.5-2.5 i would think? Anyways, if someone can tell me what I messed up or if its just time to start over I'd appreciate the help.
 
User1911
#2 Posted : 1/26/2014 2:18:59 AM
It could be a number of things causing this, from poor bark, to your solvent isnt saturated enough and other factors. I cant say excatly because that tek is just way to long to follow. CYBS Salt tek is a great tek to use with acrb.

Try adding more solvent and shaking it and letting it fully settle a good 5 or 6 times then try another pull and see what happens.
 
Entheogenerator
#3 Posted : 1/26/2014 2:32:05 AM
If your pulls aren't precipitating, you could try reducing the volume about 50% before freezing. As for the poor yield, it could be a number of things.
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