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nutmeg extract (pic) Options
 
remediosvaro
#1 Posted : 9/20/2012 10:55:20 PM
i extracted 5 grams of nutmeg into a brown thick oil, if i recrystallize in ethanol, then i will get a white powder thats very pure. anyway heres a picture of the crude extract. just outta curiosity, since the festive days are coming, if i were to infuse this onto herbs, and smoke it would it be active? im guessing most of those toxins are going to be out by recrystallization

http://www.leethacker.co...zbqms524f1d2bhs9169b.jpg
 
Garyp88
#2 Posted : 9/20/2012 11:40:05 PM
Nice. Would this be a myristicin extraction?
 
benzyme
Moderator | Skills: Analytical equipment, Chemical master expertExtreme Chemical expert | Skills: Analytical equipment, Chemical master expertChemical expert | Skills: Analytical equipment, Chemical master expertSenior Member | Skills: Analytical equipment, Chemical master expert
#3 Posted : 9/21/2012 2:15:25 AM
remediosvaro wrote:
i extracted 5 grams of nutmeg into a brown thick oil, if i recrystallize in ethanol, then i will get a white powder thats very pure.


very pure what?
what makes you think ethanol would separate out other benzodioxoles and oils?
"Nothing is true, everything is permitted." ~ hassan i sabbah
"Experiments are the only means of attaining knowledge at our disposal. The rest is poetry, imagination." -Max Planck
 
remediosvaro
#4 Posted : 9/21/2012 8:20:48 AM
benzyme, i forgot to mention, i mean recrystallization with ice cold acetone or ethanol, to remove oils and keep myristicin
 
benzyme
Moderator | Skills: Analytical equipment, Chemical master expertExtreme Chemical expert | Skills: Analytical equipment, Chemical master expertChemical expert | Skills: Analytical equipment, Chemical master expertSenior Member | Skills: Analytical equipment, Chemical master expert
#5 Posted : 9/22/2012 5:06:21 AM
I'm skeptical that an acetone/alcohol wash would leave anything pure. both elemicin and myristicin have three H-bond acceptors.
"Nothing is true, everything is permitted." ~ hassan i sabbah
"Experiments are the only means of attaining knowledge at our disposal. The rest is poetry, imagination." -Max Planck
 
Eliyahu
#6 Posted : 9/22/2012 5:43:51 AM
remediosvaro wrote:
i extracted 5 grams of nutmeg into a brown thick oil, if i recrystallize in ethanol, then i will get a white powder thats very pure. anyway heres a picture of the crude extract. just outta curiosity, since the festive days are coming, if i were to infuse this onto herbs, and smoke it would it be active? im guessing most of those toxins are going to be out by recrystallization

http://www.leethacker.co...zbqms524f1d2bhs9169b.jpg



Don't make yourself ill bro- be careful
And why do you look at the speck in your brother's eye, but do not percieve the plank in your own eye? Or how can you say to your brother, "brother let me remove the speck from your eye", when you yourself do not see the plank that is in your own eye?-Yeshua ben Yoseph
 
remediosvaro
#7 Posted : 9/22/2012 11:01:13 AM
i decided i wont consume it. but it was fun extracting anyway
 
 
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