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Number of pulls Options
 
abusedtoaster
#1 Posted : 1/25/2012 8:01:47 PM
Why wouldnt one big naphtha pull, agitated slightly more be just as productive as multiple pulls?
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Crystalito
Senior Member
#2 Posted : 1/25/2012 8:19:59 PM
Ah, excellent question!

Two words: Partition coefficient

And an amazing PPT on the issue! http://www.google.gr/url...kSDgNAjdgu7Q&cad=rja

In very few words, because more pulls are more efficient than one big pull. For example if you extract with 300 ml of naptha at once and you run the same experiment pulling thrice (3x) with 100 ml naptha, you will find that while you pulled with the same amount of solvent in both cases, the "pulling in smaller increments" method yields more!
 
abusedtoaster
#3 Posted : 1/25/2012 9:13:29 PM
Thanks!
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Dozuki
Chemical expertSenior Member
#4 Posted : 1/25/2012 10:39:20 PM
Also the alkaloids are only slightly soluble in naptha. Doing more than 3 would be recommended. It's a good re-crystallization solvent, but a poor extraction solvent for tryptamines.
 
jamie
Salvia divinorum expert | Skills: Plant growing, Ayahuasca brewing, Mushroom growingSenior Member | Skills: Plant growing, Ayahuasca brewing, Mushroom growing
#5 Posted : 1/25/2012 10:42:04 PM
warming the solvent with a double boiler helps as well I find. Be careful though and never play around with solvents and open flames etc..
Long live the unwoke.
 
amvitamine
#6 Posted : 1/25/2012 11:03:25 PM
I do multiple large pulls. 2ml solvent per gram of MHRB
 
abusedtoaster
#7 Posted : 1/26/2012 4:55:19 AM
Dozuki wrote:
It's a good re-crystallization solvent



I cant get my product to not smell like naphtha.. or even IPA if I try to cleanse, even when leaving it for over 24 hours.
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amvitamine
#8 Posted : 1/26/2012 6:43:49 PM
Bear in mind dmt has a slight plastic-y smell
 
abusedtoaster
#9 Posted : 1/27/2012 3:23:33 AM
I understand this. but mine has a slight IPA-y smell Razz
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Visty
#10 Posted : 3/4/2012 10:41:14 AM
Dozuki wrote:
Also the alkaloids are only slightly soluble in naptha. Doing more than 3 would be recommended. It's a good re-crystallization solvent, but a poor extraction solvent for tryptamines.


So you are saying that I can pull with ether, let it evaporate completely, then dissolve in naphta for freezing?
 
 
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