Hi all, I am the user Nachooo, sadly forgot my password and cant recover it, but Endlessness kindly promote this new account and have privileges again.
I live in Spain, in the Ebro valley under the Pyrenees mountains, and in the center of that big valley there are some arid zones that have mediterranean climate and some continental zones are like the iranian steppes with similar plants.
I have been going to that zones to collect wild harmala seeds for years. This zone is full of them and together with the liberty caps that grow in the mountains 100 km to the north I was able to enjoy some kind of European psilohuasca. In that zone also grow three different ephedra species (nebrodensis, fragilis and dystachia)
But some time ago I found a very good botanical text for a local researcher that cited some locations for phalaris species. Aquatica, minor, brachystachys, canariensis, paradoxa and arundinacea. The text name some explicit locations near little villages in this kind of desert zone named Los Monegros, very well know in Spain. Of all those phalaris, brachystachys was according to the text the most common and it appear in a quite large number of locations.
As I have to properly identify them and there are lots of other similar grasses here, I had to wait until the flower deveoped so I waited until early may and designed a long route in that desert with a jeep to hunt for local wild phalaris.
Sadly this year has been affected by a big drought so grasses were less and much more little than usual.. but anyway I knew that as happens with mushrooms, if you find them in bad climate conditions, when good conditions appear in the same places there will be great numbers of them.
So I started the hunt and after a few hours of driving in dusty roads I started to find the phalaris, I know the species are very similar but I think they are brachystachys cause I went to the locations were apparently only brachystachys were identified. Here are some pics of the first ones I found..they were very dry and little due to the big drough, Located in the side of very dry wheat fields under extreme heat for this time of the year.
https://imgur.com/oFgEz9Bhttps://imgur.com/sF7wcm5https://imgur.com/qyH8c0khttps://imgur.com/IIrs5pCDue to this year heat, some of them were with developed seeds. I collected lots of them and a few leaves that were still green
After this initial findings I arrived to and old unused irrigation channel were the soil was deep and with much more humidty and I found lots of plants in better condition but still very mature
https://imgur.com/JOOFUIVAfter collect some more leaves and seeds I keep my travel for a few kms and I found some Harmala plants flowering..it is so nice that the two plants grow in almost same location..
https://imgur.com/2C76N8xWhen I was returning home I pass through some irrigated fields and to my delight there was hundreds of much more greener phalaris...similar species but with the water they were much more greener and less mature..althought in flower but yet without seed..so I picked lot of leaves and marked the place in my GPS
https://imgur.com/gU4Pf02Back at home I decided to do some extractions..
Dried with a food dehydrator quickly at 70 C and I got 50 gr dry that I convert into very fine powder
I tried two approches..
I used 25 gr with a tek like Cyb´s hybrid with a defating step with naphta and then I put the solvent in the freezer waiting foe something to precipitate...but sadly I do not obtain any crystal...just some kind of very little product about 20 mg of this kind of green dust
https://imgur.com/zVTCZJTThen I slowly evaporate the naphta to find what remains in there..
This time much more product was obtained..but was a green sticky goo..
https://imgur.com/OUI1ILdThe two procuct were tested with reagents..nothing conclusive probably due to impuruties.
SO well some kind dissapointed I tried a total different approach...using the HIELO tek developed by @loveall and just decanting the water with the fridge rest instead usig drying chemicals and also using the CASEA approach. So the 25 gr that remained were extracted...
I was expecting some kind of honey like it happens with mimosa..but after three says I saw that there was no honey substance at the bottom..just tiny cristals..so I discard the EA, clean the crystals with new EA and recover the with hot destilled water to recrystallize..
To my surprise 100 mg of a very clean crystal substance with pink tones appeared
https://imgur.com/tGceUdMConsidering the plants were in full flowering mode...that was a 0,4% and they were wild phalaris..the result seems to me quite interesting and maybe extractions of these ones worth the while, specially in vegetative phase..
So I tested with some reagents...of all, Erlich and maybe Hoffman gave me some interesting result
Erlich: clearly a violet reaction
https://imgur.com/u78PtAhHoffman
https://imgur.com/4dXRPByMarquis
https://imgur.com/HDCFQHUMandelin
https://imgur.com/4yDMereMecke
https://imgur.com/i8L4k9QWell thats all...now what is need is courage to vaporize a few mgs of the results...
Hope you like the post