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Why isn’t the FB indole getting pulled?... Options
 
ThePlants
#1 Posted : 10/26/2019 9:24:27 PM
The material is Lespedeza bicolor RB.

I’m getting a strongly positive (pink) Ehrlich reaction on a water extract.
But common STB and Bufo-style extracts are completely negative with Ehrlich.

What other methods can I try for pulling the freebase?
Any suggestions are welcome, and I have plenty of material to play with. Thanks.
 
Mindlusion
Extreme Chemical expertChemical expertSenior Member
#2 Posted : 10/26/2019 9:48:50 PM
ThePlants wrote:
The material is Lespedeza bicolor RB.

I’m getting a strongly positive (pink) Ehrlich reaction on a water extract.
But common STB and Bufo-style extracts are completely negative with Ehrlich.

What other methods can I try for pulling the freebase?
Any suggestions are welcome, and I have plenty of material to play with. Thanks.


The reacting indole likely isn't an alkaloid.
Expect nothing, Receive everything.
"Experiment and extrapolation is the only means the organic chemists (humans) currrently have - in contrast to "God" (and possibly R. B. Woodward). "
He alone sees truly who sees the Absolute the same in every creature...seeing the same Absolute everywhere, he does not harm himself or others. - The Bhagavad Gita
"The most beautiful thing we can experience, is the mysterious. The source of all true art and science."
 
endlessness
Moderator
#3 Posted : 10/27/2019 12:09:54 PM
ThePlants wrote:
The material is Lespedeza bicolor RB.

I’m getting a strongly positive (pink) Ehrlich reaction on a water extract.
But common STB and Bufo-style extracts are completely negative with Ehrlich.

What other methods can I try for pulling the freebase?
Any suggestions are welcome, and I have plenty of material to play with. Thanks.


Suggestion 1 - Test it with TLC
Suggestion 2 - Prepare the different extracts and post in this thread so we can get it lab tested.

Smile
 
 
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