I did 3 1.5 hour boils on my bark, with an unmeasured amount of white vinegar each time. I don’t get crazy with the acidification, just get the ph down so the spice wants out of the bark. Then combined boils and reduced to workable amount (an 800 ml mason jar for 200 gram bark). This is when I normally jumped right to basing and forgot the defat step. So instead, I did a normal naphtha pull at this point before dmt was in freebase form. This allowed all the non polar junk that comes out later to move now while leaving spice in aqueous solution. I also froze this pull just to see if any spice came with it, but no, just a bunch of gunk. I then proceeded as normal with basing and pulling. Still a little goo, but I suspect this is the nmt and maybe a tiny bit of fats. I know you could completely defat it if you repeated the defat pull until the naphtha pulled clear, but I only did this once.
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