Hi to everyone!
Swim was doing an a/b 50g mhrb when Swim got to the freeze precipitation part.
Swim used like 50 ml naphtha to do the first pull and then evaped it to a 1/3 of the volume(like 10-15ml) and then put it in the freezer in my evap dish covered with plastic wrap, leaved it in the freezer for 24h and then poured all the naphtha in another jar leaving the dmt crystals with no more nps visible, leaved it for 10 mins out of the freezer and then all the crystals where no longer crystals, they were liquid, and then Swim decided to leave it to evap completly, leaving a layer of sticky wax and some white crystals(very small and mixed with that wax).My question here is, how do i get that crystals to stay in crystal form? And that wax is secure to vape?
-solvent evaped cleanly
-solvent was clear when pulling



Edit: forgot to say that i tried to do what says in the FAQ and still doesn't worked. Searched many info about dmt melting or resissolving but not many results.

you should of posted this if the FAQ section.

DMT is polymorphous, meaning it can take as a crystalline structure or a goo. It depends on the room temperature and or exposure to oxygen. I keep my FB crystals in freezer to solve this problem. DMT goo is just harder to weigh. if DMT oxidizes it is still smokable just a little loss of potency.

Solution to my problem was found! My solvent "naphtha 70°C-90°C" was too heavy to extract the dmt and precipitate it without forming "bubbles" of naphtha inside the xtals. Instead i used amore light naphtha "Petroleum ether 40°C-60°C" and all went good, all finally went perfect, xtals wouls form without problems and would not redissolve again, just dry white dmt powder. Also, the goo was formed because of oxigen and light exposure when the solvent was evaporating. Both solvent would leave no residue. Thanks for helping me in the chat!